RSC Publishing Logo
Perkin Transactions 1 1972-2002 logo

Year 2002
Main Index

Issue 1


Perkin 1 Abstracts: Natural Product Synthesis
Andrew Gunn Jacqueline E. Milne and Marcel de Puit
pg 1-xii; DOI:
10.1039/b110868a
PDF
Stoichiometric asymmetric processes
Simon Jones
pg 1; DOI:
10.1039/b009236n
PDF
A chemoenzymatic synthesis of the 12-membered macrolide (–)-cladospolide A
Martin G. Banwell Katrina A. Jolliffe David T. J. Loong Kenneth J. McRae and Filisaty Vounatsos
pg 22; DOI:
10.1039/b110018a
PDF
Inverse Wittig reaction of oxaphosphetenes formed by the [2+2] cycloaddition of arylphosphine oxides and dimethyl acetylenedicarboxylate (DMAD)
György Keglevich Henrietta Forintos Tamás Körtvélyesi and László Tke
pg 26; DOI:
10.1039/b108675h
PDF
Phenyl group acceleration of [1,4] carbon-to-oxygen silicon-mediated elimination–rearrangement in -silyl sulfones. Synthesis of O-silylated cinnamyl alcohols
Stefano Menichetti and Charles J. M. Stirling
pg 28; DOI:
10.1039/b109805e
PDF
Aryl H-phosphonates. Part 13. A new, general entry to aryl nucleoside phosphate and aryl nucleoside phosphorothioate diesters
Jacek Cielak Jadwiga Jankowska Micha Sobkowski Magorzata Wenska Jacek Stawiski and Adam Kraszewski
pg 31; DOI:
10.1039/b109373h
PDF
On the optical activity of the 3-aryl-4-hydroxycoumarin isolated from Millettia griffoniana: molecular modelling and total synthesis
Sébastien Combes Jean-Pierre Finet and Didier Siri
pg 38; DOI:
10.1039/b108707j
PDF
Influence of preparation procedure on polymer composition: synthesis and characterisation of polymethacrylates bearing -D-glucopyranoside and -D-galactopyranoside residues
Moira Ambrosi Andrei S. Batsanov Neil R. Cameron Benjamin G. Davis Judith A. K. Howard and Rob Hunter
pg 45; DOI:
10.1039/b108421f
PDF
Photochemical transformations of 5-halogeno-4-thiouridines
Grayna Wenska Katarzyna Taras-Goliska Katarzyna Lamparska-Kupsik Bohdan Skalski Maria Gdaniec and Zofia Gdaniec
pg 53; DOI:
10.1039/b108380e
PDF
Cascade radical synthesis of heteroarenes via iminyl radicals
W. Russell Bowman Colin F. Bridge Philip Brookes Martin O. Cloonan and David C. Leach
pg 58; DOI:
10.1039/b108323f
PDF
4-Phenyloxazolidin-2-ones and isoindolin-1-ones: chiral auxiliaries for Diels–Alder reactions of N-substituted 1,3-dienes
Helena McAlonan James P. Murphy Mark Nieuwenhuyzen Karen Reynolds Pakala K. S. Sarma Paul J. Stevenson and Norris Thompson
pg 69; DOI:
10.1039/b108059h
PDF
Diastereocontrolled synthesis of hydroxylated lactams
Mark. D. Andrews Andrew G. Brewster and Mark G. Moloney
pg 80; DOI:
10.1039/b108056n
PDF
Synthesis of soluble halogenated aryloxy substituted indium phthalocyanines
M. John Plater Adam Jeremiah and Grant Bourhill
pg 91; DOI:
10.1039/b107689m
PDF
Reductive cleavage of N-substituted aromatic amides as tert-butyl acylcarbamates
Ulf Ragnarsson Leif Grehn Hernani L. S. Maia and Luis S. Monteiro
pg 97; DOI:
10.1039/b107330n
PDF
The effect of oxygen on the regioselectivity in the rhodium catalysed hydrosilylation of 1,3-dienes
Magnus Gustafsson and Torbjörn Frejd
pg 102; DOI:
10.1039/b106143g
PDF
Controlled stepwise conversion of 2,4,6,8-tetrachloropyrimido[5,4-d]pyrimidine into 2,4,6,8-tetrasubstituted pyrimido[5,4-d]pyrimidines
Julian S. Northen F. Thomas Boyle William Clegg Nicola J. Curtin Andrew J. Edwards Roger J. Griffin and Bernard T. Golding
pg 108; DOI:
10.1039/b102224p
PDF
The asymmetric Bischler–Napieralski reaction: preparation of 1,3,4-trisubstituted 1,2,3,4-tetrahydroisoquinolines
Marcello Nicoletti David O'Hagan and Alexandra M. Z. Slawin
pg 116; DOI:
10.1039/b106942j
PDF

Issue 2


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Alexis Carstairs Ian Jackson Denise McIntyre Alan Watt Sabine Flitsch and Nicholas Turner
pg 2-vii; DOI:
10.1039/b111338k
PDF
Photolabile protecting groups and linkers
Christian G. Bochet
pg 125; DOI:
10.1039/b009522m
PDF
Synthesis of nornicotine, nicotine and other functionalised derivatives using solid-supported reagents and scavengers
Ian R. Baxendale Gloria Brusotti Masato Matsuoka and Steven V. Ley
pg 143; DOI:
10.1039/b109482n
PDF
Use of a modified ring-switching strategy to synthesise the glutamate antagonist (2S)-2-amino-3-(2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)propionate and related compounds with two chiral centres
Andrew Dinsmore Paul M. Doyle and Douglas W. Young
pg 155; DOI:
10.1039/b109820a
PDF
Metal triflates catalyzed efficient synthesis of 3,4-dihydro-2H-1-benzopyrans
Jhillu S. Yadav Basi V. Subba Reddy M. Aruna Chenna Venugopal T. Ramalingam S. Kiran Kumar and Ajit C. Kunwar
pg 165; DOI:
10.1039/b109538m
PDF
-Methylene tetrazole-based peptidomimetics: synthesis and inhibition of HIV protease
Barnaby C. H. May and Andrew D. Abell
pg 172; DOI:
10.1039/b109128j
PDF
Stereochemical considerations on the stereoselective cyclopropanation reactions of 3-aryl-2-phosphonoacrylates induced by the (–)-8-phenylmenthyl group as a chiral auxiliary
Ryukichi Takagi Miki Hashizume Minoru Nakamura Shahnaz Begum Yoshikazu Hiraga Satoshi Kojima and Katsuo Ohkata
pg 179; DOI:
10.1039/b108925k
PDF
Two novel racemic synthetic approaches to LTB4 and LTB3 methyl esters
Christine Gauthier Dominique Castet Yvan Ramondenc and Gérard Plé
pg 191; DOI:
10.1039/b108847e
PDF
Design and synthesis of N-nonpolar nucleobase dipeptides: application of the Ugi reaction for the preparation of dipeptides having fluoroarylalkyl groups appended to the nitrogen atom
Biplab Kumar Das Norio Shibata and Yoshio Takeuchi
pg 197; DOI:
10.1039/b108760f
PDF
Regioselective synthesis of pyrazoles via the ring cleavage of 3-substituted N-alkylated 3-hydroxyisoindolin-1-ones
Kyu-Tae Chang Yong Hyun Choi Seung-Ho Kim Yong-Jin Yoon and Woo Song Lee
pg 207; DOI:
10.1039/b108485m
PDF
Synthesis and alkylation reaction of 1-arylmethyleneamino- and 1-arylsulfonyl-5-hydroxy-1H-1,2,3-triazoles
Yury A. Rozin Elena A. Savel'eva Yury Yu. Morzherin Wim Dehaen Suzanne Toppet Luc Van Meervelt and Vasily A. Bakulev
pg 211; DOI:
10.1039/b108202g
PDF
Synthesis of 6-alkyl analogues of the 1-azabicyclo[4.3.0]nonan-2-one system by a strategy of geminal acylation and Beckmann rearrangement
Christine E. Elliott David O. Miller and D. Jean Burnell
pg 217; DOI:
10.1039/b108164k
PDF
Cleavage of cyclopropyl ketones mediated by alkylmercury(II) hydrides
Pablo H. Di Chenna Andrés Ferrara Alberto A. Ghini and Gerardo Burton
pg 227; DOI:
10.1039/b107258g
PDF
Probing the mechanism of loss of carbon-20 in gibberellin biosynthesis. Synthesis of gibberellin 3,20-hemiacetal and 19,20-lactol analogues and their metabolism by a recombinant GA 20-oxidase
Jane L. Ward Paul Gaskin Robert G. S. Brown Graham S. Jackson Peter Hedden Andy L. Phillips Christine L. Willis and Michael H. Beale
pg 232; DOI:
10.1039/b106990j
PDF
Parasite glycoconjugates. Part 12. Synthesis of deoxy, fluorodeoxy and aminodeoxy disaccharide phosphates, substrate analogues for the elongating -D-mannopyranosylphosphate transferase in the Leishmania
Dmitry V. Yashunsky Yury E. Tsvetkov Michael A. J. Ferguson and Andrei V. Nikolaev
pg 242; DOI:
10.1039/b106182h
PDF
Kinetic resolution of amines with enantiopure 3-N,N-diacylaminoquinazolin-4(3H)-ones
Abdullah G. Al-Sehemi Robert S. Atkinson and John Fawcett
pg 257; DOI:
10.1039/b105917n
PDF

Issue 3


Perkin 1 Abstracts: Natural Product Synthesis
Andrew Gunn Jacqueline E. Milne Marcel de Puit and Duncan McArthur
pg 3-ix; DOI:
10.1039/b200355b
PDF
-Oxy sulfones and sulfoximines: versatile intermediates
Fabrice Chemla
pg 275; DOI:
10.1039/b009523k
PDF
Synthesis of the first amine–cyanocarboxyboranes, isoelectronic analogues of -cyanocarboxylic acids
Béla Györi Zoltán Berente Róbert Király and István Lázár
pg 300; DOI:
10.1039/b111682g
PDF
Facile synthesis of disubstituted and spiro five-membered benzosultams mediated by TMSCl–NaI–MeCN reagent
Zhaopeng Liu Norio Shibata and Yoshio Takeuchi
pg 302; DOI:
10.1039/b109832b
PDF
Preparation of 1-phenylcyclohexa-2,5-diene-1-carboxylates and their use in free-radical mediated syntheses
Paul A. Baguley Leon V. Jackson and John C. Walton
pg 304; DOI:
10.1039/b110527m
PDF
Synthesis of novel cyclophanes containing both benzo[1,2-b:5,4-b]difuran and naphthalene rings
Kwanghee Koh Park Hongsan Lim Sun-Hyuk Kim and Dae Hyun Bae
pg 310; DOI:
10.1039/b110312a
PDF
Reaction of Herz salts with malononitrile: a general route to (6H-1,2,3-benzodithiazol-6-ylidene)malononitriles
Panayiotis A. Koutentis and Charles W. Rees
pg 315; DOI:
10.1039/b110024f
PDF
Making conjugated connections to porphyrins: a comparison of alkyne, alkene, imine and azo links
Thomas E. O. Screen Iain M. Blake Leigh H. Rees William Clegg Simon J. Borwick and Harry L. Anderson
pg 320; DOI:
10.1039/b109915a
PDF
Thionation of bisindole derivatives with P4S10 or elemental sulfur
Tomasz Janosik Jan Bergman Birgitta Stensland and Claes Stålhandske
pg 330; DOI:
10.1039/b109840c
PDF
N- and O-Alkylation of isoquinolin-1-ones in the Mitsunobu reaction: development of potential drug delivery systems
Sandra Ferrer Declan P. Naughton Ifat Parveen and Michael D. Threadgill
pg 335; DOI:
10.1039/b109776h
PDF
Reaction of diimines and azines with diphenylcyclopropenone
Mohsen Abdel-Motaal Gomaa
pg 341; DOI:
10.1039/b109711n
PDF
Photoinduced [2+2] cycloadditions (the Paterno–Bchi reaction) of 1-acetylisatin with enol ethers—regioselectivity, diastereoselectivity and acid catalysed transformations of the spirooxetane products
Yan Zhang Jie Xue Yi Gao Hoong-Kun Fun and Jian-Hua Xu
pg 345; DOI:
10.1039/b109697d
PDF
Unsymmetrical O-bridged calixarenes derived from tBu-calix[4]arene and p-benzylcalix[4]arene
Mohamed Makha Peter J. Nichols Michaele J. Hardie and Colin L. Raston
pg 354; DOI:
10.1039/b109625g
PDF
Diastereoselective electrophilic substitution of -amino-substituted benzylic organometallics
Ugo Azzena
pg 360; DOI:
10.1039/b109633h
PDF
Intramolecular Diels–Alder reaction of cyclopenta-1,3-diene derivatives generated in situ from 4-(pent-4-enyl)cyclopent-2-enone ethylene ketals
Masakazu Ohkita Hidetoshi Kawai and Takashi Tsuji
pg 366; DOI:
10.1039/b109614a
PDF
Efficient syntheses of 6-prenylcoumarins and linear pyranocoumarins: Total synthesis of suberosin, toddaculin, O-methylapigravin (O-methylbrosiperin), O-methylbalsamiferone, dihydroxanthyletin, xanthyletin and luvangetin
Raghao S. Mali Priya P. Joshi Paramjeet Kaur Sandhu and Anita Manekar-Tilve
pg 371; DOI:
10.1039/b109597h
PDF
7-Mesityl-2,2-dimethylindan-1-ol: a novel alcohol which serves as both a chiral auxiliary and a protective group for carboxy functions
Eiji Koshiishi Tetsutaro Hattori Naoki Ichihara and Sotaro Miyano
pg 377; DOI:
10.1039/b109396g
PDF
Regio- and stereoselective synthesis of fluoroalkenes and fluoroalkadienes
Masanori Yoshida Daisuke Ota Tsuyoshi Fukuhara Norihiko Yoneda and Shoji Hara
pg 384; DOI:
10.1039/b108796g
PDF
Superiority of the carbamoylmethyl ester as an acyl donor for the kinetically controlled amide-bond formation mediated by -chymotrypsin
Toshifumi Miyazawa Eiichi Ensatsu Nobuhiro Yabuuchi Ryoji Yanagihara and Takashi Yamada
pg 390; DOI:
10.1039/b108735p
PDF
-Chymotrypsin-catalysed segment condensations via the kinetically controlled approach using carbamoylmethyl esters as acyl donors in organic media
Toshifumi Miyazawa Eiichi Ensatsu Makoto Hiramatsu Ryoji Yanagihara and Takashi Yamada
pg 396; DOI:
10.1039/b108738j
PDF
Flash vacuum pyrolysis over magnesium. Part 1. Pyrolysis of benzylic, other aryl/alkyl and aliphatic halides
R. Alan Aitken Philip K. G. Hodgson John J. Morrison and Adebayo O. Oyewale
pg 402; DOI:
10.1039/b108663d
PDF
Asymmetric transfer hydrogenation of ketones using amino alcohol and monotosylated diamine derivatives of indane
Matthew J. Palmer Jennifer A. Kenny Tim Walsgrove Aparecida M. Kawamoto and Martin Wills
pg 416; DOI:
10.1039/b108538g
PDF
Regioselective acylation of 1-hydroxypyrazoles via metalated intermediates
Niels Østergaard Niels Skjærbæk Mikael Begtrup and Per Vedsø
pg 428; DOI:
10.1039/b107850j
PDF
Reactions of trimethylsilyl-derived iodohydrins with electron-rich -systems
Eti Ishai Sarit Shamai and Ben-Ami Feit
pg 434; DOI:
10.1039/b105233k
PDF
Phosphabenzenes as electron withdrawing phosphine ligands in catalysis
Erin F. DiMauro and Marisa C. Kozlowski
pg 439; DOI:
10.1039/b101454o
PDF

Issue 4


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 4-vii; DOI:
10.1039/b200808b
PDF
Applications of stoichiometric transition metal complexes in organic synthesis
Ross Fryatt and Steven D. R. Christie
pg 447; DOI:
10.1039/b101946p
PDF
Palladium-catalyzed coupling reaction of acylzirconocene chlorides with hypervalent iodonium salts: synthesis of aryl-substituted ketones
Suk-Ku Kang and Seok-Keun Yoon
pg 459; DOI:
10.1039/b110983a
PDF
Boronic acid appended azo dyes–colour sensors for saccharides
Christopher J. Ward Prakash Patel and Tony D. James
pg 462; DOI:
10.1039/b108896c
PDF
Synthesis of 5-arylpyrrolo[1,2-c]pyrimidin-1(2H)-ones
Mercedes Álvarez David Fernández and John A. Joule
pg 471; DOI:
10.1039/b111142f
PDF
Exploitation of chemical predisposition in synthesis: an approach to the manzamenones
Saleh Al-Busafi Jeremy R. Doncaster Michael G. B. Drew Andrew C. Regan and Roger C. Whitehead
pg 476; DOI:
10.1039/b110829h
PDF
Synthesis and nucleic-acid-binding properties of sulfamide- and 3-N-sulfamate-modified DNA
Kevin J. Fettes Nigel Howard David T. Hickman Steven Adah Mark R. Player Paul F. Torrence and Jason Micklefield
pg 485; DOI:
10.1039/b110603c
PDF
A useful enantioselective synthesis of chroman-2-ylmethanol
Jean-Yves Goujon Alexis Duval and Bernard Kirschleger
pg 496; DOI:
10.1039/b110578g
PDF
Extremely simple and practical synthesis of ()-vertinolide via the Michael addition
Kunihiko Takabe Nobuyuki Mase Masaru Nomoto Masanori Daicho Tetsuo Tauchi and Hidemi Yoda
pg 500; DOI:
10.1039/b110460h
PDF
Solution-phase combinatorial synthesis using multicomponent Grignard reagents
Xifu Liang and Mikael Bols
pg 503; DOI:
10.1039/b109952n
PDF
Substitution of -azido ethers with Grignard reagents and its use in combinatorial chemistry
Mukulesh Baruah and Mikael Bols
pg 509; DOI:
10.1039/b110428b
PDF
Intramolecular addition of acyldiazenecarboxylates onto double bonds in the synthesis of heterocycles
José V. Prata Dina-Telma S. Clemente Sundaresan Prabhakar Ana M. Lobo Isabel Mourato (in part) and Paula S. Branco (in part)
pg 513; DOI:
10.1039/b110414d
PDF
Synthetic approaches to 1-(2-chlorophenyl)isoquinoline-3-carboxylic acid
Yves L. Janin Emmanuel Roulland Arnaud Beurdeley-Thomas Didier Decaudin Claude Monneret and Marie-France Poupon
pg 529; DOI:
10.1039/b110301f
PDF
Flash vacuum pyrolysis of stabilised phosphorus ylides. Part 17. Preparation of aliphatic amino acid derived -alkoxycarbonylamino--oxo ylides and pyrolysis to give ,-acetylenic -amino acid and GABA analogues
R. Alan Aitken Nazira Karodia Tracy Massil and Robert J. Young
pg 533; DOI:
10.1039/b110243e
PDF
Structure of the dimers arising from one-electron electrochemical reduction of pyridinium salts 3,5-disubstituted with electron-withdrawing groups
Vincenzo Carelli Felice Liberatore Silvano Tortorella Barbara Di Rienzo and Luigi Scipione
pg 542; DOI:
10.1039/b110140b
PDF
3-Hydroxypyrroles and 1H-pyrrol-3(2H)-ones. Part 14. Pyrolysis of oxazolidinylmethylene derivatives of Meldrum's acid – synthesis of N-alkenyl-3-hydroxypyrroles and related reactions
Abd El-Aal M. Gaber Gordon A. Hunter and Hamish McNab
pg 548; DOI:
10.1039/b109788a
PDF
Control of the reaction between 2-aminobenzothiazoles and Mannich bases. Synthesis of pyrido[2,1-b][1,3]benzothiazoles versus [1,3]benzothiazolo[2,3-b]quinazolines
Jairo Quiroga Pedro Hernández Braulio Insuasty Rodrigo Abonía Justo Cobo Adolfo Sánchez Manuel Nogueras and John N. Low
pg 555; DOI:
10.1039/b109676a
PDF
Synthesis and chiroptical properties of pseudocolchicine and neocolchicine, novel unnatural regioisomers of colchicine
Marino Cavazza Maurizio Zandomeneghi and Francesco Pietra
pg 560; DOI:
10.1039/b109075p
PDF
Convergent synthesis of the spiroketal core of the HIV-1 protease inhibitors the didemnaketals
Yanxing Jia Xin Li Pingzhen Wang Bin Wu Xuezhi Zhao and Yongqiang Tu
pg 565; DOI:
10.1039/b108512n
PDF
Staudinger reactions of unsymmetrical cyclic ketenes: a synthetically useful approach to spiro -lactams and derivatives. Reaction mechanism and theoretical studies
Eduardo Alonso Carlos del Pozo and Javier González
pg 571; DOI:
10.1039/b103279h
PDF

Issue 5


Professor K. C. Nicolaou*
K.C. Nicolaou
pg 5-vii; DOI:
10.1039/b200756h
PDF
Perkin 1 Abstracts: Natural Product Synthesis
Andrew Gunn Jacqueline E. Milne Marcel de Puit and Duncan McArthur
pg 5-xi; DOI:
10.1039/b201458k
PDF
Efficient stereoselective synthesis of peptidomimetics containing hydroxyethylamine dipeptide isosteres utilizing the aza-Payne rearrangement and O, N-acyl transfer reactions
Hirokazu Tamamura Tadakazu Hori Akira Otaka and Nobutaka Fujii
pg 577; DOI:
10.1039/b200324b
PDF
Arylated pyridines: Suzuki reactions of O-substituted 2,6-dihalogenated-3-hydroxypyridines
Glen M. Chapman Stephen P. Stanforth Brian Tarbit and Michael D. Watson
pg 581; DOI:
10.1039/b111620g
PDF
The first enantioselective total synthesis of cyclomyltaylane-5-ol and determination of its absolute stereochemistry
Hisahiro Hagiwara Hitoshi Sakai Takashi Uchiyama Yoshiaki Ito Noriyuki Morita Takashi Hoshi Toshio Suzuki and Masayoshi Ando
pg 583; DOI:
10.1039/b111594b
PDF
Convenient syntheses of 2,3,4,5-tetrahydro-1,4-benzothiazepines, -1,4-benzoxazepines and -1,4-benzodiazepines
Alan R. Katritzky Yong-Jiang Xu and Hai-Ying He
pg 592; DOI:
10.1039/b111296c
PDF
Synthesis and chemical reactivity of methoxycarbonyl-1,3-dioxinyl(pivaloyl)ketene—a persistent -oxoketene
Bianca C. Wallfisch Ferdinand Belaj Curt Wentrup C. Oliver Kappe and Gert Kollenz
pg 599; DOI:
10.1039/b111143d
PDF
Studies on tellurium-containing heterocycles. Part 18. Preparation and structure of 2-benzotelluropyrylium salts and 2-benzoselenopyrylium salts
Haruki Sashida Kazuo Ohyanagi Mao Minoura and Kin-ya Akiba
pg 606; DOI:
10.1039/b111045b
PDF
Synthesis of homochiral amino acid pyrazine and pyrrole analogues of glutamate antagonists
Andrew Dinsmore Paul M. Doyle Matthias Steger and Douglas W. Young
pg 613; DOI:
10.1039/b110979k
PDF
An approach to 2,3-dihydropyrroles and -iodopyrroles based on 5-endo-dig cyclisations
David W. Knight Adele L. Redfern and Jeremy Gilmore
pg 622; DOI:
10.1039/b110751h
PDF
A new method for the polymer-supported synthesis of cyclic oligoesters for potential applications in macrocyclic lactone synthesis and combinatorial chemistry
Clare L. Ruddick Philip Hodge Anthony Cook and Andrew J. McRiner
pg 629; DOI:
10.1039/b110528k
PDF
Arabinose-derived bicyclic amino acids: synthesis, conformational analysis and construction of an v3-selective RGD peptide
Francesco Peri Roberta Bassetti Enrico Caneva Luca de Gioia Barbara La Ferla Marco Presta Elena Tanghetti and Francesco Nicotra
pg 638; DOI:
10.1039/b110453e
PDF
Novel, cyclic and bicyclic 1,3-diols as catalysts for the diethylzinc addition to aldehydes
Ian Sarvary Yiqian Wan and Torbjörn Frejd
pg 645; DOI:
10.1039/b110082n
PDF
Facile synthesis of 2-substituted ethyl 2-(2-amino-5-ethoxycarbonylthiazol-4-yl)ethanoates
Diana Brikut Frank A. Sløk Christian Rømming and Algirdas akus
pg 652; DOI:
10.1039/b110022j
PDF
Synthesis of 2,16- and 4,16-difluoroestradiols and their 11-methoxy derivatives as potential estrogen receptor-binding radiopharmaceuticals
Yann Seimbille Hasrat Ali and Johan E. van Lier
pg 657; DOI:
10.1039/b110021c
PDF
Ring-opening reactions of cyclopropanes. Part 7. Selenenylation and cyanoselenenylation of ethyl 2,2-dimethoxycyclopropanecarboxylates
M. Liliana Graziano M. Rosaria Iesce Flavio Cermola Giovanni Caputo and Fulvio De Lorenzo
pg 664; DOI:
10.1039/b109480g
PDF
endo-Selective allylation at the benzylic centre of a Cr(CO)3 complexed aromatic ring
Sunil K. Mandal and Amitabha Sarkar
pg 669; DOI:
10.1039/b109291j
PDF
,-Didehydroamino acid derivatives with an isoxazolyl or a pyrazolyl moiety: The effect of substituents and reaction conditions on their stereoselective formation from 2H-pyran-2-ones
Lidija Vraniar Anton Meden Slovenko Polanc and Marijan Koevar
pg 675; DOI:
10.1039/b107624h
PDF
Preparation of novel O-sulfated amino acid building blocks with improved acid stability for Fmoc-based solid-phase peptide synthesis
Socorro Vázquez Campos Les P. Miranda and Morten Meldal
pg 682; DOI:
10.1039/b107320f
PDF
Stereochemical and electronic features of the [3 + 2] cycloaddition of pentafulvenes with acylnitrones
Francis Djapa Kabula Ciamala Jean-Marie Melot Joel Vebrel and Guillaume Herlem
pg 687; DOI:
10.1039/b106892j
PDF
A straightforward synthesis of some fused aza-arenes via nucleophilic displacement of a ring hydrogen atom in nitroarenes by aromatic hydrazone anions
Koji Uehata Takehiko Kawakami and Hitomi Suzuki
pg 696; DOI:
10.1039/b105230f
PDF
Book Reviews

pg 703; DOI:
10.1039/b200424k
PDF

Issue 6


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 6-ix; DOI:
10.1039/b201816k
PDF
New synthesis of ,-diiodoalkynes and capped iodobutadiynes
Jaromír Hlavatý Ladislav Kavan and Martin tícha
pg 705; DOI:
10.1039/b201360f
PDF
Regioselective reduction of maleimide and citraconimide derivatives: general preparation of 5-hydroxy-1,5-dihydropyrrol-2-one
Nobuyuki Mase Toshiki Nishi Masaomi Hiyoshi Kazuhiro Ichihara Junichiro Bessho Hidemi Yoda and Kunihiko Takabe
pg 707; DOI:
10.1039/b200729k
PDF
Synthesis of (2E)-4-hydroxy-3-methylbut-2-enyl diphosphate, a key intermediate in the biosynthesis of isoprenoids
Jane L. Ward and Michael H. Beale
pg 710; DOI:
10.1039/b200712f
PDF
A novel spiroketalization reaction of 1,7-dihydroxyhepta-2,5-diyn-4-ones
Koichi Tanaka and Naoyuki Harada
pg 713; DOI:
10.1039/b200215a
PDF
Synthesis of the first superstructured chiral corrole
Bruno Andrioletti and Eric Rose
pg 715; DOI:
10.1039/b200188h
PDF
The preparation of thiophene-based azacryptand Mannich bases
Julie D. E. Chaffin John M. Barker and Patrick R. Huddleston
pg 717; DOI:
10.1039/b200479h
PDF
Double stereodifferentiation in aldol reactions of pyroglutamic urethane esters
Bernard A. Starkmann and Douglas W. Young
pg 725; DOI:
10.1039/b200443g
PDF
Synthesis of 2-substituted indolines using sequential Pd-catalyzed processes
Hervé J. C. Deboves Christopher Hunter and Richard F. W. Jackson
pg 733; DOI:
10.1039/b200163b
PDF
Reactions of acyl chlorides with LiAlHSeH. Preparation of diacyl selenides, diacyl diselenides, selenocarboxylates and cyclic selenoanhydrides
Mamoru Koketsu Futoshi Nada Sohma Hiramatsu and Hideharu Ishihara
pg 737; DOI:
10.1039/b200147k
PDF
Efficient regioselective synthesis of triheterocyclic compounds: imidazo[2,1-b]benzothiazoles, pyrimido[2,1-b]benzothiazolones and pyrimido[2,1-b]benzothiazoles
Cyrille Landreau David Deniaud Michel Evain Alain Reliquet and Jean-Claude Meslin
pg 741; DOI:
10.1039/b111639h
PDF
Dendritic encapsulation of amino acid–metal complexes. Synthesis and studies of dendron-functionalized L-tyrosine–metal (ZnII, CoII) complexes
Thatavarathy Rama Krishna and Narayanaswamy Jayaraman
pg 746; DOI:
10.1039/b110188a
PDF
Application of [5+2] cycloaddition toward the functionalized bicyclo[4.3.1]decane ring system: synthetic study of phomoidride B (CP-263,114)
Naoki Ohmori
pg 755; DOI:
10.1039/b110607b
PDF
Synthetic and mechanistic study of the acid-promoted aromatisation of the Diels–Alder adduct: 6,7-dimethoxy-1-(4-pyridyl)-1,4-epoxytetrahydronaphthalene-2,3-dicarboxylate
Masakatsu Sugahara Yasunori Moritani Tooru Kuroda Kazuhiko Kondo and Tatsuzo Ukita
pg 768; DOI:
10.1039/b110265f
PDF
Tandem sigmatropic shifts in [4 + 2] cycloaddition reactions of 1,3-diazabuta-1,3-dienes with butadienylketene: synthesis of pyrimidinone derivatives
Arun K. Sharma S. Jayakumar Maninder S. Hundal and Mohinder P. Mahajan
pg 774; DOI:
10.1039/b109922c
PDF
A facile and simple entry into isodideoxynucleosides
Angshuman Chattopadhyay and Avinash Salaskar
pg 785; DOI:
10.1039/b109785g
PDF
Synthesis of quinoxaline derivatives from substituted acetanilides through intramolecular quaternization reactions
Sonia de Castro Roberto Chicharro and Vicente J. Arán
pg 790; DOI:
10.1039/b109725c
PDF
Modular fluorescence sensors for saccharides
Susumu Arimori Michael L. Bell Chan S. Oh Karine A. Frimat and Tony D. James
pg 803; DOI:
10.1039/b108998f
PDF
Insights on the synthesis and organisational phenomena of twisted pyrazine–pyridine hybrids
Fenton Heirtzler Markus Neuburger and Klaus Kulike
pg 809; DOI:
10.1039/b107751a
PDF
An efficient synthesis of the four mono methylated isomers of (+)-catechin including the major metabolites and of some dimethylated and trimethylated analogues through selective protection of the catechol ring
Cécile Cren-Olivé Stéphane Lebrun and Christian Rolando
pg 821; DOI:
10.1039/b107340k
PDF
Novel glucocorticoid antedrugs possessing a 21-(-lactone) ring
Richard M. Angell Keith Biggadike Rosanne M. Farrell Stephen S. Flack Ashley P. Hancock Wendy R. Irving Sean M. Lynn and Panayiotis A. Procopiou
pg 831; DOI:
10.1039/b200190j
PDF

Issue 7


Perkin 1 Abstracts: Solid Phase Organic Synthesis
Andrew Gunn Stephen McAteer and Marcel de Puit
pg 7-vii; DOI:
10.1039/b202398a
PDF
Synthetic receptors for carboxylic acids and carboxylates
Richard J. Fitzmaurice Graham M. Kyne David Douheret and Jeremy D. Kilburn
pg 841; DOI:
10.1039/b009041g
PDF
Alkali metal ion selectivities of podands that form pseudo-cyclic structures by intramolecular hydrogen bonding
Yoichi Habata Yoji Fukuda Sadatoshi Akabori and Jerald S. Bradshaw
pg 865; DOI:
10.1039/b201525k
PDF
Highly enantioselective epoxidation of unfunctionalized olefins catalyzed by a novel recyclable chiral poly-salen–Mn(III) complex
Yuming Song Xiaoquan Yao Huilin Chen Guizhi Pan Xinquan Hu and Zhuo Zheng
pg 870; DOI:
10.1039/b201294b
PDF
The use of -allyltricarbonyliron lactone complexes in the synthesis of the resorcylic macrolides - and -zearalenol
Svenja Burckhardt and Steven V. Ley
pg 874; DOI:
10.1039/b201164f
PDF
Olefination of aromatic ketones: synthesis of mono- and dihaloalkenes
Vasily N. Korotchenko Alexey V. Shastin Valentine G. Nenajdenko and Elisabeth S. Balenkova
pg 883; DOI:
10.1039/b201131j
PDF
Resolution and configurational assignment of 3,4,5,6-tetrahydro-2-methyl-2,6-methano-2H-1-benzoxocine derivatives
Tibor Kurtán Eszter Baitz-Gács Zsuzsa Májer Attila Bényei and Sándor Antus
pg 888; DOI:
10.1039/b200751g
PDF
Total synthesis of bisabolane sesquiterpenoids, -bisabol-1-one, curcumene, curcuphenol and elvirol: utility of catalytic enamine reaction in cyclohexenone synthesis
Hisahiro Hagiwara Tomoyuki Okabe Hiroki Ono Vijayendra P. Kamat Takashi Hoshi Toshio Suzuki and Masayoshi Ando
pg 895; DOI:
10.1039/b200629b
PDF
Atroposelectivity in the electrophilic substitution reactions of laterally lithiated and silylated tertiary amides
Jonathan Clayden Jennifer H. Pink Neil Westlund and Christopher S. Frampton
pg 901; DOI:
10.1039/b200358a
PDF
Synthesis of cholic acid-based molecular receptors: head-to-head cholaphanes
Pramod S. Pandey Roopali Rai and Rhiddi B. Singh
pg 918; DOI:
10.1039/b200320c
PDF
Synthesis of ABE tricyclic analogues of methyllycaconitine using a Wacker oxidation–aldol strategy to append the B ring to the AE fragment
David Barker Margaret A. Brimble Malcolm McLeod G. Paul Savage and David J. Wong
pg 924; DOI:
10.1039/b200073n
PDF
Synthesis, characterisation and application of lanthanide cyclen complexes in organic synthesis
Andrei S. Batsanov James I. Bruce Thota Ganesh Paul J. Low Ritu Kataky Horst Puschmann and Patrick G. Steel
pg 932; DOI:
10.1039/b111628b
PDF
Pigments of fungi. Part 68. Synthesis and absolute configuration of thysanone
Christopher D. Donner and Melvyn Gill
pg 938; DOI:
10.1039/b111446h
PDF
Enantioselective total synthesis of vicenistatin, a novel 20-membered macrocyclic lactam antitumor antibiotic
Yoshitaka Matsushima Hiroaki Itoh Takuya Nakayama Sayo Horiuchi Tadashi Eguchi and Katsumi Kakinuma
pg 949; DOI:
10.1039/b111146a
PDF
Stereoselectivity in ring-closing olefin metathesis (RCM) of tethered dihexenoyl derivatives
Mitsuhiro Arisawa Hiroaki Kaneko Atsushi Nishida and Masako Nakagawa
pg 959; DOI:
10.1039/b111122c
PDF
Synthesis of 2,5-dihydrofurans via alkylidene carbene insertion reactions
Louise F. Walker Ahmed Bourghida Stephen Connolly and Martin Wills
pg 965; DOI:
10.1039/b111097g
PDF
Molecular recognition of modified nucleobases. Self-complementarity and base-pairing of betainic guanine model compounds
Andreas Schmidt Nikoloz Kobakhidze and Markus Karl Kindermann
pg 982; DOI:
10.1039/b110318k
PDF
A facile route to poly[1-(2,4,6-trichlorophenyl)-1H-1,2,4-triazol-5-yl]alkane derivatives
Quanrui Wang Haiyan Yang Yi Liu Zongbiao Ding and Fenggang Tao
pg 991; DOI:
10.1039/b110059a
PDF

Issue 8


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 8-vii; DOI:
10.1039/b202864f
PDF
Polyene natural products
Carl Thirsk and Andrew Whiting
pg 999; DOI:
10.1039/b109741p
PDF
The simultaneous use of immobilised reagents for the one-pot conversion of alcohols to carboxylic acids
Kosuke Yasuda and Steven V. Ley
pg 1024; DOI:
10.1039/b201776h
PDF
An exceptionally simple and catalytic method for regeneration of carbonyl functionality from the corresponding 1,3-oxathiolanes
Ejabul Mondal Priti Rani Sahu Gopal Bose and Abu T. Khan
pg 1026; DOI:
10.1039/b110305a
PDF
Synthesis and in vitro enzyme activity of an oxa analogue of azi-DAP
Russell J. Cox Jeremy Durston and David I. Roper
pg 1029; DOI:
10.1039/b201727j
PDF
Self-terminating, oxidative radical cyclizations of medium-sized cycloalkynones with inorganic and organic oxygen-centered radicals of type XO: the reaction pathway depends on the nature of X
Uta Wille and Christian Jargstorff
pg 1036; DOI:
10.1039/b201672a
PDF
A convenient preparation of several N-linked glycoamino acid building blocks for efficient solid-phase synthesis of glycopeptides
Jeroen van Ameijde H. Bauke Albada and Rob M. J. Liskamp
pg 1042; DOI:
10.1039/b201296k
PDF
Synthesis of enantiomerically pure divinyl- and diallylcarbinols
Bernd Schmidt and Holger Wildemann
pg 1050; DOI:
10.1039/b200976e
PDF
Total synthesis of naamine C and pyronaamidine, antitumor marine imidazole alkaloids
Seikou Nakamura Ikuo Kawasaki Miki Kunimura Miyuki Matsui Yoko Noma Masayuki Yamashita and Shunsaku Ohta
pg 1061; DOI:
10.1039/b200845a
PDF
Synthesis and biological evaluation of a PtdIns(4,5)P2 and a phosphatidic acid affinity matrix
Ze-Yi Lim Jan W. Thuring Andrew B. Holmes Maria Manifava and Nicholas T. Ktistakis
pg 1067; DOI:
10.1039/b200585a
PDF
Diastereoselective addition of chiral azomethine ylides to cyclic ,-unsaturated N-enoylbornanesultams
Staffan Karlsson and Hans-Erik Högberg
pg 1076; DOI:
10.1039/b200579d
PDF
Approaches to the synthesis of (2R,3S)-2-hydroxymethylpyrrolidin-3-ol (CYB-3) and its C(3) epimer: a cautionary tale
Alison N. Hulme and Karen S. Curley
pg 1083; DOI:
10.1039/b200415a
PDF
Novel uridin-2-yl carbamates: synthesis, incorporation into oligodeoxyribonucleotides, and remarkable fluorescence properties of 2-pyren-1-ylmethylcarbamate
Vladimir A. Korshun Dmitry A. Stetsenko and Michael J. Gait
pg 1092; DOI:
10.1039/b111434b
PDF
Intramolecular acceleration effect of a tosylamide group on the electrochemical oxidation of N--silylalkyl amides
Tohru Kamada and Akira Oku
pg 1105; DOI:
10.1039/b111106j
PDF
Screening of yeast species for the stereo-selective reduction of bicyclo[2.2.2]octane-2,6-dione
Adriana L. Botes Daniel Harvig Martha S. van Dyk Ian Sarvary Torbjörn Frejd Mikael Katz Bärbel Hahn-Hägerdal and Marie F. Gorwa-Grauslund
pg 1111; DOI:
10.1039/b111064k
PDF
Regiocontrolled synthesis of the macrocyclic polyamine alkaloid ()-lunarine, a time-dependent inhibitor of trypanothione reductase
Chris J. Hamilton Alan H. Fairlamb and Ian M. Eggleston
pg 1115; DOI:
10.1039/b110149h
PDF
Synthesis of glycero amino acid-based surfactants. Part 2. Lipase-catalysed synthesis of 1-O-lauroyl-rac-glycero-3-O-(N-acetyl-L-amino acid) and 1,2-di-O-lauroyl-rac-glycero-3-O-(N-acetyl-L-amino acid) derivatives
Carmen Morán María Rosa Infante and Pere Clapés
pg 1124; DOI:
10.1039/b200577h
PDF
Electrochemical synthesis of a pyridinium-conjugated assembly based on nucleophilic substitution of oligothiophene -radical cation
Yi Li Kaori Kamata Tadashi Kawai Jiro Abe and Tomokazu Iyoda
pg 1135; DOI:
10.1039/b200738j
PDF

Issue 9


Perkin 1 Abstracts: Solid Phase Organic Synthesis
Fabrice Anizon Jennifer Delaney Andrew Gunn Hassan Mamdani Catherine McCusker Fiona McKerlie and Tanya Wildman
pg 9-v; DOI:
10.1039/b203347j
PDF
Recent developments in the chemistry of dihydropyridines
Rodolfo Lavilla
pg 1141; DOI:
10.1039/b101371h
PDF
Tin(II) chloride mediated allylation of aldimines generated in situ with allylstannane in water
Takahiko Akiyama and Yuji Onuma
pg 1157; DOI:
10.1039/b202486a
PDF
The reaction of dialkoxytitanacyclopropanes and dialkoxytitanacyclopropenes with carbon dioxide
Yvan Six
pg 1159; DOI:
10.1039/b201527g
PDF
Deoxygenation of tertiary and secondary alcohols ROH by thiol-catalysed radical-chain redox decomposition of derivatives ROCH2X to give RH and XCHO
Hai-Shan Dang and Brian P. Roberts
pg 1161; DOI:
10.1039/b202411j
PDF
Distorted electron acceptors: an unexpected reaction involving tetramethyl-TCNQ
Norman A. Bell David J. Crouch Lawrence R. H. High Derek J. Simmonds Simon J. Coles and Michael B. Hursthouse
pg 1171; DOI:
10.1039/b201862b
PDF
Synthesis, X-ray crystal structures and Horner–Wittig addition reactions of some protected -aminophosphine oxides
Neil Feeder David J. Fox Jonathan A. Medlock and Stuart Warren
pg 1175; DOI:
10.1039/b201680j
PDF
Parallel synthesis of new phenylalanino-2-(phenylthio)pyrrolidin-3-one scaffold-based analogues
Gilles Quéléver Martin Bouygues and Jean-Louis Kraus
pg 1181; DOI:
10.1039/b201147f
PDF
Synthesis and investigation of L-fuco- and D-glucurono-azafagomine
Henrik H. Jensen Astrid Jensen Rita G. Hazell and Mikael Bols
pg 1190; DOI:
10.1039/b200884j
PDF
Synthesis of (1S,2R)-1-phenyl-2-[(S)-1-aminoalkyl]-N,N-diethylcyclopropanecarboxamides as novel NMDA receptor antagonists having a unique NMDA receptor subtype selectivity
Yuji Kazuta Ryuichi Tsujita Shigeo Uchino Noriko Kamiyama Daisuke Mochizuki Kanako Yamashita Yutaka Ohmori Akitake Yamashita Tamotsu Yamamoto Shinich Kohsaka Akira Matsuda and Satoshi Shuto
pg 1199; DOI:
10.1039/b111540p
PDF
Structural effects on sigmatropic shifts in heteroaromatic allyl ethers
Nuna C. P. Araújo Pedro M. M. Barroca Jamie F. Bickley Amadeu F. Brigas M. Lurdes S. Cristiano Robert A. W. Johnstone Rui M. S. Loureiro and Paula C. A. Pena
pg 1213; DOI:
10.1039/b102674g
PDF
Book Reviews

pg 1220; DOI:
10.1039/b202565p
PDF

Issue 10


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 10-vii; DOI:
10.1039/b203807m
PDF
Efficient and chemoselective cleavage of TBS ethers by a sub-stoichiometric amount of decaborane
Yeon Joo Jeong Ji Hee Lee Eun Soo Park and Cheol Min Yoon
pg 1223; DOI:
10.1039/b201794f
PDF
Synthesis of a linear bis-porphyrin with a Ru(phen)22+-complexed 2,2-bipyridine spacer
James I. Bruce Jean-Claude Chambron Philipp Kölle and Jean-Pierre Sauvage
pg 1226; DOI:
10.1039/b202407c
PDF
Synthesis of fluorinated 2-phenyl-4-quinolones from pyrrole-2,3-diones
V. V. Ramana Rao and Curt Wentrup
pg 1232; DOI:
10.1039/b202128e
PDF
Reactions of 1,2,3-dithiazoles with halogenated malononitriles
Irene C. Christoforou Panayiotis A. Koutentis and Charles W. Rees
pg 1236; DOI:
10.1039/b202038f
PDF
Synthesis and evaluation of sulfonium analogues of isofucofagomine as glycosidase inhibitors
Víctor Ulgar José G. Fernández-Bolaños and Mikael Bols
pg 1242; DOI:
10.1039/b202021c
PDF
Solid phase synthesis of C2,N6-disubstituted adenosine analogues
Boris Rodenko Martin J. Wanner and Gerrit-Jan Koomen
pg 1247; DOI:
10.1039/b201943d
PDF
Aminolysis of cyclic thioxocarbonate of (R,R)-di-tert-butyl tartrate: efficient access to thio- and thiolcarbamates
Ludovic Faissat Claude Chavis Jean-Louis Montéro and Marc Lucas
pg 1253; DOI:
10.1039/b201691e
PDF
Novel heterocycles containing the pyrazole unit
Jan Svtlík and Tibor Liptaj
pg 1260; DOI:
10.1039/b201529n
PDF
Synthesis and analysis of peptide nucleic acid oligomers using Fmoc/acyl-protected monomers
Györgyi Kovács Zoltán Timár Zoltán Kupihár Zoltán Kele and Lajos Kovács
pg 1266; DOI:
10.1039/b201297a
PDF
Synthesis of S-thioacyl dithiophosphates, efficient and chemoselective thioacylating agents
Leszek Doszczak and Janusz Rachon
pg 1271; DOI:
10.1039/b201233b
PDF
Solvent-free chelation-assisted hydroacylation of olefin by rhodium(I) catalyst under microwave irradiation
André Loupy Saber Chatti Sarah Delamare Dae-Yon Lee Jong-Hwa Chung and Chul-Ho Jun
pg 1280; DOI:
10.1039/b200442a
PDF
Synthesis of chiral organotin reagents: synthesis of enantiomerically enriched bicyclo[2.2.1]hept-2-yl tin hydrides from camphor. X-Ray crystal structures of (dimethyl)[(1R,2S,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-2-yl]tin chloride and methyl(phenyl)bis[(1R,2S,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-2-yl]stannane
Madeleine Helliwell Eric J. Thomas and Linda A. Townsend
pg 1286; DOI:
10.1039/b200317c
PDF
Investigation of the base promoted tandem syn-elimination–Favorskii rearrangement of levoglucosan sulfonates
Lene Muldgaard Ib B. Thomsen Rita G. Hazell and Mikael Bols
pg 1297; DOI:
10.1039/b200064b
PDF
In vitro fluorine-19 nuclear magnetic resonance study of the liberation of antitumor nitrogen mustard from prodrugs
Frédéric Schmidt and Claude Monneret
pg 1302; DOI:
10.1039/b111549a
PDF
Efficient synthesis of -substituted -haloenones by rhodium(II)-catalyzed and thermal reactions of iodonium ylides
Yong Rok Lee and Yong Ug Jung
pg 1309; DOI:
10.1039/b111206f
PDF
Indium-mediated diastereoselective allylation reactions: preparation of -hydroxy and -amino acids
Jung Gyu Lee Kyung Il Choi Ae Nim Pae Hun Yeong Koh Yonghan Kang and Yong Seo Cho
pg 1314; DOI:
10.1039/b110505c
PDF
A convenient general synthesis of 3-substituted 2H-chromene derivatives
Perry T Kaye and Xolani W. Nocanda
pg 1318; DOI:
10.1039/b201827f
PDF

Issue 11


Perkin 1 Abstracts: Natural Product Synthesis
Andrew Gunn Stephen McAteer Jacqueline E. Milne and Marcel de Puit
pg 11-ix; DOI:
10.1039/b204498f
PDF
Boron acids as protective agents and catalysts in synthesis
Peter J. Duggan and Edward M. Tyndall
pg 1325; DOI:
10.1039/b006767i
PDF
Rapid and convergent assembly of the polycyclic framework assigned to the cytotoxic marine alkaloid halitulin
Martin G. Banwell Andrew M. Bray Alison J. Edwards and David J. Wong
pg 1340; DOI:
10.1039/b111401h
PDF
Synthetic studies on CP-225,917 and CP-263,114: concise synthesis of the bicyclic core using an intramolecular Mukaiyama aldol reaction
Alan Armstrong Trevor J. Critchley Marie-Edith Gourdel-Martin Richard D. Kelsey and Andrew A. Mortlock
pg 1344; DOI:
10.1039/b202752f
PDF
Synthesis of pseudoxazolones and their inhibition of the 3C cysteine proteinases from hepatitis A virus and human rhinovirus-14
Yeeman K. Ramtohul Nathaniel I. Martin Lara Silkin Michael N. G. James and John C. Vederas
pg 1351; DOI:
10.1039/b202643k
PDF
Intramolecular Michael-type addition of azadienes to 1,4-naphthoquinones instead of Aza-Diels–Alder cycloaddition: a synthesis of ascididemin
Juan M. Cuerva Diego J. Cárdenas and Antonio M. Echavarren
pg 1360; DOI:
10.1039/b202555h
PDF
Quinolizine-2,4-diones by reversible dimerisation 2-pyridylketenes
Carsten Plüg Arvid Kuhn and Curt Wentrup
pg 1366; DOI:
10.1039/b202523j
PDF
Preparation of (+)-nemorensic acid and approaches to nemorensine using the partial reduction of electron deficient furans
Timothy J. Donohoe Jean-Baptiste Guillermin and Daryl S. Walter
pg 1369; DOI:
10.1039/b202514k
PDF
Carbohydrate-derived thiols as protic polarity-reversal catalysts for enantioselective radical-chain reactions
Yudong Cai Brian P. Roberts and Derek A. Tocher
pg 1376; DOI:
10.1039/b202022j
PDF
Stereocontrolled synthesis of acyclic terpenoids viaN-ylide [2,3]rearrangement of ammonium salts with the stereodefined isoprene unit
Kiyoshi Honda Masayuki Tabuchi Hiroki Kurokawa Masatoshi Asami and Seiichi Inoue
pg 1387; DOI:
10.1039/b201304e
PDF
Synthesis of unsymmetrically substituted meso-phenylporphyrins by Suzuki cross coupling reactions
Baolu Shi and Ross W. Boyle
pg 1397; DOI:
10.1039/b201622b
PDF
Elemental iodine catalyzed [4 + 2] cycloaddition reactions of o-quinomethanes: an efficient synthesis of trans-fused pyrano[3,2-c]benzopyrans
Jhillu Singh Yadav Basi V. Subba Reddy C. Venkateswara Rao and K. Vishweshwar Rao
pg 1401; DOI:
10.1039/b200193b
PDF
Symmetrical and inherently chiral water-soluble calix[4]arenes bearing dihydroxyphosphoryl groups
Maxim A. Tairov Myroslav O. Vysotsky Olga I. Kalchenko Vladimir V. Pirozhenko and Vitaly I. Kalchenko
pg 1405; DOI:
10.1039/b110691k
PDF

Issue 12


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 12-vii; DOI:
10.1039/b204941b
PDF
The first isolation and characterization of sulfonylbuta-1,3-diynes
Mitsuhiro Yoshimatsu Kasumi Oh-Ishi Genzoh Tanabe and Osamu Muraoka
pg 1413; DOI:
10.1039/b203913n
PDF
Synthesis and light absorption/emission properties of novel bis-squaraine dyes with extensively conjugated -electron systems
Shigeyuki Yagi Shin Murayama Yutaka Hyodo Yoshihiko Fujie Msahiko Hirose and Hiroyuki Nakazumi
pg 1417; DOI:
10.1039/b203793a
PDF
The role of the carbonyl group in the intermolecular 1,3-cycloaddition of azido(2-heteroaryl)methanones with activated olefins
Paolo Zanirato
pg 1420; DOI:
10.1039/b203577d
PDF
Carbanion induced synthesis of annulated unsymmetrical biaryls through ring transformation of 2H-pyran-2-one
Vishnu Ji Ram Nidhi Agarwal Abhishek S. Saxena Farhanullah Ashoke Sharon and Prakas R. Maulik
pg 1426; DOI:
10.1039/b203544h
PDF
A new entry to 9-azabicyclo[3.3.1]nonanes using radical translocation/cyclisation reactions of 2-(but-3-ynyl)-1-(o-iodobenzoyl)piperidines
Tatsunori Sato Taro Yamazaki Yumi Nakanishi Jun-ichi Uenishi and Masazumi Ikeda
pg 1438; DOI:
10.1039/b203243k
PDF
Towards complete stereochemical control: complementary methods for the synthesis of six diastereoisomeric monosaccharide mimetics
Robert Hodgson Tahir Majid and Adam Nelson
pg 1444; DOI:
10.1039/b202890e
PDF
Synthesis of some 3,4-dihydro-2H-benzo[f]pyrano[2,3-h]chromen-6-one derivatives
Demetrios N. Nicolaides Daman R. Gautam Konstantinos E. Litinas and Theodora Papamehael
pg 1455; DOI:
10.1039/b202640f
PDF
Tributyltin hydride-mediated radical cyclisation of carbonyls to form functionalised oxygen and nitrogen heterocycles
Jon Bentley Paul A. Nilsson and Andrew F. Parsons
pg 1461; DOI:
10.1039/b202077g
PDF
Chemical reactivity of hydroxymethylnaphthols: hetero-Diels–Alder products of o-naphthoquinomethides derived from 2- and 3-hydroxymethylnaphthols
Muhammad Ashram David O. Miller and Paris E. Georghiou
pg 1470; DOI:
10.1039/b200893a
PDF
Synthesis of (E)- and (Z)-29-methylidyne-2,3-oxidosqualene derivatives as inhibitors of liver and yeast oxidosqualene cyclase
Maurizio Ceruti Franca Viola Gianni Balliano Paola Milla Giorgio Roma Giancarlo Grossi and Flavio Rocco
pg 1477; DOI:
10.1039/b200888m
PDF
Reaction of -carbanion of imines with N-tosylimines: a facile route to -aminoaldehydes and 1,3-diamines
Xue-Long Hou Yu-Mei Luo Ke Yuan and Li-Xin Dai
pg 1487; DOI:
10.1039/b200198e
PDF
Direct NH-aziridination of ,-unsaturated ketones
Jiaxi Xu and Peng Jiao
pg 1491; DOI:
10.1039/b200046f
PDF
Nitrone dipolar cycloaddition routes to piperidines and indolizidines. Part 9. Formal synthesis of (–)-pinidine and total synthesis of (–)-histrionicotoxin, (+)-histrionicotoxin and (–)-histrionicotoxin 235A
Edwin C. Davison Martin E. Fox Andrew B. Holmes Stephen D. Roughley Catherine J. Smith Geoffrey M. Williams John E. Davies Paul R. Raithby Joseph P. Adams Ian T. Forbes Neil J. Press and Mervyn J. Thompson
pg 1494; DOI:
10.1039/b200328g
PDF

Issue 13


Efficient synthesis of functionalized 3H-pyrrolo[1,2-a]indoles
Issa Yavari Mehdi Adib and Mohammad H. Sayahi
pg 1517; DOI:
10.1039/b204433c
PDF
Catalysis by ionic liquids: solvent-free efficient transthioacetalisation of acetals by molten tetrabutylammonium bromide
Brindaban C. Ranu Arijit Das and Sampak Samanta
pg 1520; DOI:
10.1039/b204363g
PDF
High surface area polystyrene resin-supported Pt catalysts in room temperature solventless octene hydrosilylation using methyldichlorosilane
Robert Drake David C. Sherrington and Steven J. Thomson
pg 1523; DOI:
10.1039/b203899d
PDF
Conversion of tetrazoles into hydrazonoyl chlorides. Novel donor–dithiazolium interactions
Charles W. Rees Sivaprasad Sivadasan Andrew J. P. White and David J. Williams
pg 1535; DOI:
10.1039/b202211g
PDF
Synthesis of 1,3,4-thiadiazole oligomers
Van-Duc Le Charles W. Rees and Sivaprasad Sivadasan
pg 1543; DOI:
10.1039/b203705j
PDF
Palladium(II) complex-catalysed enantioselective benzoylation of alcohols using carbon monoxide and an organobismuth(V) compound
Tomochika Iwata Yoshihiro Miyake Yoshiaki Nishibayashi and Sakae Uemura
pg 1548; DOI:
10.1039/b203465d
PDF
Conversion of (Z)-1,4-dihydroxyalk-2-enes into 2,5-dihydrofurans and of alkane-1,4-diols into tetrahydrofurans via acid-catalysed cyclisation of the monoisoureas formed by their copper(I)-mediated reactions with dicyclohexylcarbodiimide
Michael G. Duffy and David H. Grayson
pg 1555; DOI:
10.1039/b203389p
PDF
Expeditious preparation of various 9-6a,10a cis and trans 2-substituted tetrahydrocannabinoids
Jean-Yves Goujon Françoise Zammattio and Bernard Kirschleger
pg 1564; DOI:
10.1039/b203366f
PDF
Synthesis of diselenadiazafulvalenes and influence of steric strain on their anodic behavior
Zdenko asar Ivan Leban Alenka Majcen-Le Maréchal and Dominique Lorcy
pg 1568; DOI:
10.1039/b203317h
PDF
Reaction of 5-halo-1,2,3-thiadiazoles with arylenediamines as a new approach to tricyclic 1,3,6-thiadiazepines
Natalya N. Volkova Evgeniy V. Tarasov Luc Van Meervelt Suzanne Toppet Wim Dehaen and Vasiliy A. Bakulev
pg 1574; DOI:
10.1039/b203072a
PDF
Carotenoids and related polyenes. Part 8. Total synthesis of optically active mytiloxanthin applying the stereoselective rearrangement of tetrasubstituted epoxide
Chisato Tode Yumiko Yamano and Masayoshi Ito
pg 1581; DOI:
10.1039/b201228f
PDF
Synthesis of pyrazole and pyrimidine Trger's-base analogues
Rodrigo Abonia Andrea Albornoz Hector Larrahondo Jairo Quiroga Braulio Insuasty Henry Insuasty Angelina Hormaza Adolfo Sánchez and Manuel Nogueras
pg 1588; DOI:
10.1039/b200862a
PDF
Novel photoadditions of tertiary amines to the -position of ,-unsaturated ,-epoxy nitriles
Keitaro Ishii Satoshi Hakamada Mayumi Nagano Masahiro Noji Shigeo Sugiyama Masashi Kotera and Masanori Sakamoto
pg 1592; DOI:
10.1039/b110372e
PDF
Book Reviews

pg 1599; DOI:
10.1039/b205252k
PDF

Issue 14


Perkin 1 Abstracts: Natural Product Synthesis
Andrew Gunn Stephen McAteer Jacqueline E. Milne and Marcel de Puit
pg 14-x; DOI:
10.1039/b205788n
PDF
Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 14-vii; DOI:
10.1039/b206029a
PDF
Annulenes, 1980–2000
Robert D. Kennedy Douglas Lloyd and Hamish McNab
pg 1601; DOI:
10.1039/b109576p
PDF
A chemoenzymatic synthesis of the styryllactone (+)-goniodiol from naphthalene
Martin G. Banwell Mark J. Coster Ochitha P. Karunaratne and Jason A. Smith
pg 1622; DOI:
10.1039/b205230j
PDF
Synthesis and biological evaluation of phospholane and dihydrophosphole analogues of the glutamate receptor agonist AP4
Stuart J. Conway Jacqueline C. Miller Andrew D. Bond Barry P. Clark and David E. Jane
pg 1625; DOI:
10.1039/b204891d
PDF
Unprecedented 1,3-dipolar cycloaddition of azomethine ylides to ester carbonyl
Mikhail S. Novikov Igor V. Voznyi Alexander F. Khlebnikov Jürgen Kopf and Rafael R. Kostikov
pg 1628; DOI:
10.1039/b204464a
PDF
Desymmetrisation of meso difuryl alcohols, diols and their derivatives: complementary directed and undirected asymmetric dihydroxylation reactions
Robert Hodgson Tahir Majid and Adam Nelson
pg 1631; DOI:
10.1039/b204904j
PDF
Streptomyces coelicolor phosphopantetheinyl transferase: a promiscuous activator of polyketide and fatty acid synthase acyl carrier proteins
Russell J. Cox John Crosby Oliver Daltrop Frank Glod Malgorzata E. Jarzabek Thomas P. Nicholson Michelle Reed Thomas J. Simpson Leah H. Smith Florilène Soulas Anna E. Szafranska and James Westcott
pg 1644; DOI:
10.1039/b204633b
PDF
Synthesis of chiral oxazolidin-2-ones from N-alkoxycarbonyl amino epoxides: a computational study
F. Javier Casado-Bellver M. Eugenia González-Rosende Amparo Asensio J. Miquel Jordá-Gregori Angeles Alvarez-Sorolla José Sepúlveda-Arques Mario Orena and Roberta Galeazzi
pg 1650; DOI:
10.1039/b203702e
PDF
Synthesis and antiviral evaluation of novel conformationally locked nucleosides and masked 5-phosphate derivatives thereof
Torsten Bryld Marianne H. Sørensen Poul Nielsen Troels Koch Claus Nielsen and Jesper Wengel
pg 1655; DOI:
10.1039/b203484k
PDF
Synthesis of tetrasubstituted pyridines by the acid-catalysed Bohlmann–Rahtz reaction
Mark C. Bagley Christian Brace James W. Dale Maren Ohnesorge Nathan G. Phillips Xin Xiong and Justin Bower
pg 1663; DOI:
10.1039/b203397f
PDF
N–H Insertion reactions of rhodium carbenoids. Part 3. The development of a modified Bischler indole synthesis and a new protecting-group strategy for indoles
Katherine E. Bashford Anthony L. Cooper Peter D. Kane Christopher J. Moody Sendogagounder Muthusamy and Elizabeth Swann
pg 1672; DOI:
10.1039/b202666j
PDF
Novel trichloroindolizine derivatives via intramolecular acylation of a bis(chloroacyl)bipyridine
Najat Sam Sghir Elkadiri Hubert Le Bozec Loic Toupet Maria Daoudi Najib Bitit Taibi Ben Hadda and Pierre H. Dixneuf
pg 1688; DOI:
10.1039/b202616n
PDF
Studies towards the total synthesis of solanoeclepin A: synthesis of the 7-oxabicyclo[2.2.1]heptane moiety and attempted seven-membered ring formation
Jorg C. J. Benningshof Richard H. Blaauw Angeline E. van Ginkel Jan H. van Maarseveen Floris P. J. T. Rutjes and Henk Hiemstra
pg 1693; DOI:
10.1039/b201987f
PDF
Studies towards the total synthesis of solanoeclepin A: synthesis and potato cyst nematode hatching activity of analogues containing the tetracyclic left-hand substructure
Jorg C. J. Benningshof Maarten IJsselstijn Sabine R. Wallner Anne L. Koster Richard H. Blaauw Angeline E. van Ginkel Jean-François Brière Jan H. van Maarseveen Floris P. J. T. Rutjes and Henk Hiemstra
pg 1701; DOI:
10.1039/b202020n
PDF
Thioester analogues of peptidoglycan fragment MurNAc-L-Ala--D-Glu as substrates for peptidoglycan hydrolase MurNAc-L-Ala amidase
Ross L. Harding Joanne Henshaw Joannah Tilling and Timothy D. H. Bugg
pg 1714; DOI:
10.1039/b200921h
PDF
Synthesis and binding properties of chiral macrocyclic barbiturate receptors: application to nitrile oxide cyclizations
Brian S. Rasmussen Unai Elezcano and Troels Skrydstrup
pg 1723; DOI:
10.1039/b110865b
PDF

Issue 15


Perkin 1 Abstracts: Natural Product Synthesis
Andrew Gunn Stephen McAteer Jacqueline E. Milne and Marcel de Puit
pg 15-vii; DOI:
10.1039/b206710m
PDF
The emergence of the cyclopentenone prostaglandins as important, biologically active compounds
Stanley M. Roberts M. Gabriella Santoro and Eugene S. Sickle
pg 1735; DOI:
10.1039/b110043m
PDF
C-Glycoside formation via Lewis acid promoted reaction of O-glycosylimidates with pyrroles
David J. Armitt Martin G. Banwell Craig Freeman and Christopher R. Parish
pg 1743; DOI:
10.1039/b205690a
PDF
Acid catalysed rearrangement of a spiroketal enol ether. An easy synthesis of chrycorin
Biao-Lin Yin Yikang Wu and Yu-Lin Wu
pg 1746; DOI:
10.1039/b205229f
PDF
Partial reduction of 3-heteroatom substituted 2-furoic acids: the role of an ortho group in viability and stereoselectivity
Timothy J. Donohoe Andrew A. Calabrese Jean-Baptiste Guillermin Christopher. S. Frampton and Daryl Walter
pg 1748; DOI:
10.1039/b203437a
PDF
The [2,3] sigmatropic rearrangement of N-benzyl-O-allylhydroxylamines
Stephen G. Davies John F. Fox Simon Jones Anne J. Price Miguel A. Sanz Thomas G. R. Sellers Andrew D. Smith and Fátima C. Teixeira
pg 1757; DOI:
10.1039/b205323n
PDF
Microwave assisted facile synthesis of Elvirol, Curcuphenol and Sesquichamaenol using Montmorillonite K-10 clay in dry media
Vasundhara Singh Anupam Khurana Irvinder Kaur Varinder Sapehiyia Goverdhan L. Kad and Jasvinder Singh
pg 1766; DOI:
10.1039/b204509p
PDF
Heteroaryl radicals. Part 1. Synthesis of linear pyridine-fused ring systems by endo-selective 2-pyridyl radical cyclizations
Sarbendu Maiti Basudeb Achari Ranjan Mukhopadhyay and Asish Kr. Banerjee
pg 1769; DOI:
10.1039/b204436f
PDF
NMR characterisation of five isomeric ,-diformyl-meso-tetraphenylporphyrins
Ana M. G. Silva Maria A. F. Faustino Tânia M. P. C. Silva Maria G. P. M. S. Neves Augusto C. Tomé Artur M. S. Silva and José A. S. Cavaleiro
pg 1774; DOI:
10.1039/b203850a
PDF
Regio- and stereocontrolled synthesis of 2-5 linked phosphorothioate oligoadenylates by uranyl ion catalyst in aqueous solution
Masamitu Shimazu Kazuo Shinozuka and Hiroaki Sawai
pg 1778; DOI:
10.1039/b203707f
PDF
Regio- and stereoselective ring-opening of chiral 1,3-oxazolidin-2-one derivatives by organocopper reagents provides novel access to di-, tri- and tetra-substituted alkene dipeptide isosteres
Shinya Oishi Ayumu Niida Takae Kamano Yoshihisa Miwa Tooru Taga Yoshihiko Odagaki Nobuyuki Hamanaka Mikio Yamamoto Keiichi Ajito Hirokazu Tamamura Akira Otaka and Nobutaka Fujii
pg 1786; DOI:
10.1039/b203482d
PDF
The Diels–Alder reactivity of (E)-3-phenylsulfonylprop-2-enenitrile, a cyanoacetylene equivalent
Pamela J. Bradley and David H. Grayson
pg 1794; DOI:
10.1039/b203391g
PDF
Synthesis of 2,3-didehydro-2,3-dideoxy-2-fluoro apionucleosides as potential antiviral agents
Hyung Ryong Moon Hea Ok Kim and Lak Shin Jeong
pg 1800; DOI:
10.1039/b203126d
PDF
Synthesis, reactivity and conformational preferences of novel enediynyl peptides: a possible scaffold for -sheet capping turns
Amit Basak Kakali Rani Rudra Subhendu Sekhar Bag and Ajoy Basak
pg 1805; DOI:
10.1039/b202660k
PDF
Synthesis and lipase catalysed stereoselective acylation of some 3-methylalkan-2-ols, identified as sex pheromone precursors in females of pine sawfly species
Erik Hedenström Helen Edlund Susan Lund Malin Abersten and David Persson
pg 1810; DOI:
10.1039/b201395a
PDF
Hybrid compounds generated by the introduction of a nogalamycin-producing plasmid into Streptomyces argillaceus
Tero Kunnari Karel D. Klika Gloria Blanco Carmen Méndez Pekka Mäntsälä Juha Hakala Reijo Sillanpää Petri Tähtinen Jose Salas and Kristiina Ylihonko
pg 1818; DOI:
10.1039/b200444p
PDF
Irreversible photoisomerization behavior of 2-stilbazole covalently bound to porphyrin
Hiroshi Sugimoto Keigo Kuramoto and Shohei Inoue
pg 1826; DOI:
10.1039/b109377k
PDF

Issue 16


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 16-vii; DOI:
10.1039/b207223h
PDF
Chiral 2,2-bipyridines: ligands for asymmetric induction
Nicholas C. Fletcher
pg 1831; DOI:
10.1039/b204272j
PDF
First synthesis of 25,26-bridged thiacalix[4]crowns by the use of a 25,26-O-disiloxanediyl-capped p-tert-butylthiacalix[4]arene
Fumitaka Narumi Nobuji Matsumura Naoya Morohashi Hiroshi Kameyama and Sotaro Miyano
pg 1843; DOI:
10.1039/b206050g
PDF
A novel one pot synthesis of nitrogen containing heterocycles: an alternate methodology to the Biginelli and Hantzsch reactions
Mazaahir Kidwai Shilpi Saxena Richa Mohan and R. Venkataramanan
pg 1845; DOI:
10.1039/b205539m
PDF
Some regioselective cross-coupling reactions of halopyridines and halopyrimidines
Nadja M. Simkovsky Monika Ermann Stanley M. Roberts David M. Parry and Andy D. Baxter
pg 1847; DOI:
10.1039/b205027g
PDF
A concise synthesis of carpanone using solid-supported reagents and scavengers
Ian R. Baxendale Ai-Lan Lee and Steven V. Ley
pg 1850; DOI:
10.1039/b203388g
PDF
Asymmetric synthesis of -pyridyl--amino acid derivatives
Steven D. Bull Stephen G. Davies David. J. Fox Massimo Gianotti Peter M. Kelly Camille Pierres Edward D. Savory and Andrew D. Smith
pg 1858; DOI:
10.1039/b204653a
PDF
N-Acyl Quat pyrrolidinone auxiliary as a chiral amide equivalent via direct aminolysis
Stephen G. Davies and Darren J. Dixon
pg 1869; DOI:
10.1039/b205326h
PDF
A new synthesis of temozolomide
Martin J. Wanner and Gerrit-Jan Koomen
pg 1877; DOI:
10.1039/b205614c
PDF
New chiral pyrazine-based ligands for self-assembly reactions
Thomas Bark Helen Stoeckli-Evans and Alexander von Zelewsky
pg 1881; DOI:
10.1039/b205563p
PDF
Efficient synthesis of N-(trifluoromethylsulfonyl)trifluoromethanesulfonimidoyl fluoride – the key agent in the preparation of compounds with superstrong electron-withdrawing groups and strong acidic properties
Romute Yu. Garlyauskayte Andrey V. Bezdudny Christophe Michot Michel Armand Yurii L. Yagupolskii and Lev M. Yagupolskii
pg 1887; DOI:
10.1039/b205169a
PDF
A straightforward synthesis of DAH (3-deoxy-D-arabino-hept-2-ulosonic acid) and DRH (3-deoxy-D-ribo-hept-2-ulosonic acid)
Ke-Gang Liu Shou-Gang Hu Yikang Wu Zhu-Jun Yao and Yu-Lin Wu
pg 1890; DOI:
10.1039/b205047a
PDF
Preparation and Stille cross-coupling reaction of the first organotin reagents of azulenes. Easy access to poly(azulen-6-yl)benzene derivatives
Shunji Ito Tetsuo Okujima and Noboru Morita
pg 1896; DOI:
10.1039/b203836f
PDF
Synthetic transformation of hydroxymatairesinol from Norway spruce (Picea abies) to 7-hydroxysecoisolariciresinol, (+)-lariciresinol and (+)-cyclolariciresinol
Patrik Eklund Reijo Sillanpää and Rainer Sjöholm
pg 1906; DOI:
10.1039/b202493d
PDF
Diastereoselective synthesis of aziridines from (1R)-10-(N,N-dialkylsulfamoyl)isobornyl 2H-azirine-3-carboxylates
Yolanda S. P. Álvares M. José Alves Nuno G. Azoia Jamie F. Bickley and Thomas L. Gilchrist
pg 1911; DOI:
10.1039/b202321k
PDF

Issue 17


Perkin 1 Abstracts: Natural Product Synthesis
Andrew Gunn Stephen McAteer Jacqueline E. Milne and Marcel de Puit
pg 17-vii; DOI:
10.1039/b207912g
PDF
Rapid analogue syntheses of heteroaromatic compounds
Ian Collins
pg 1921; DOI:
10.1039/b108580h
PDF
First synthesis of phosphatidylcholine and cholesteryl derivatives bearing an unsaturated aldehyde residue
Arnold N. Onyango Teruhiko Nitoda Takao Kaneko Mitsuyoshi Matsuo Shuhei Nakajima and Naomichi Baba
pg 1941; DOI:
10.1039/b206231n
PDF
Condensations of thiophene with ketones
Brian J. Morrison and Oliver C. Musgrave
pg 1944; DOI:
10.1039/b205484c
PDF
Lipase-catalyzed resolution and desymmetrization of 2-hydroxymethylaziridines
Paolo Davoli Emilia Caselli Maria Bucciarelli Arrigo Forni Giovanni Torre and Fabio Prati
pg 1948; DOI:
10.1039/b205374h
PDF
Synthesis of functionalised macrocyclic compounds as Na+ and K+ receptors: a mild and high yielding nitration in water of mono and bis 2-methoxyaniline functionalised crown ethers
Thorfinnur Gunnlaugsson H. Q. Nimal Gunaratne Mark Nieuwenhuyzen and Joseph P. Leonard
pg 1954; DOI:
10.1039/b205299g
PDF
Synthesis and functionalization of thiophene congeners of Trger's base
Tomoshige Kobayashi Takashi Moriwaki Masaya Tsubakiyama and Shihori Yoshida
pg 1963; DOI:
10.1039/b205227j
PDF
Synthesis of 2-aryl-2H,4H-imidazo[4,5-d][1,2,3]triazoles from triethyl N-(1-ethyl-2-methyl-4-nitro-1H-imidazol-5-yl)phosphorimidate by reaction with aryl isocyanates
Abutariq Taher Sandra Eichenseher Alexandra M. Z. Slawin George Tennant and George W. Weaver
pg 1968; DOI:
10.1039/b205216b
PDF
Chemoenzymic synthesis of oligosaccharide fragments of the capsular polysaccharide of Streptococcus pneumoniae type 14
Dirk Michalik Johannes F. G. Vliegenthart and Johannis P. Kamerling
pg 1973; DOI:
10.1039/b204933c
PDF
Complex tetrahydrofurans from carbohydrate lactones: THF amino acids as building blocks for unnatural biopolymers
Daniel D. Long Martin D. Smith Angeles Martín Joseph R. Wheatley David G. Watkin Mattaius Müller and George W. J. Fleet
pg 1982; DOI:
10.1039/b111258a
PDF
On the steric acceleration of ene reactions
Nandeo Choony Nikolai Kuhnert Peter G. Sammes Graham Smith and Robert W. Ward
pg 1999; DOI:
10.1039/b204778k
PDF
Carotenoids and related polyenes. Part 9. Total synthesis of thermozeaxanthin and thermocryptoxanthin and the stabilizing effect of thermozeaxanthin on liposomes
Yumiko Yamano Yoshitsugu Sakai Masayuki Hara and Masayoshi Ito
pg 2006; DOI:
10.1039/b204011p
PDF
The azomethine ylide strategy for -lactam synthesis. Azapenams and 1-azacephams
David Brown Giles A. Brown Mark Andrews Jonathan M. Large Dominique Urban Craig P. Butts Neil J. Hales and Timothy Gallagher
pg 2014; DOI:
10.1039/b203890k
PDF
Synthesis and crystal structure of [26,27-2H6] 24-epi-cathasterone
Adelheid Kolbe Petra Fuchs Andrea Porzel Ute Baumeister Alfred Kolbe and Günter Adam
pg 2022; DOI:
10.1039/b203323b
PDF
Book Reviews

pg 2028; DOI:
10.1039/b206722f
PDF

Issue 18


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 18-vii; DOI:
10.1039/b208231b
PDF
Diiodosamarium based polymerisations
Seema Agarwal and Andreas Greiner
pg 2033; DOI:
10.1039/b203903f
PDF
The chalcogeno-Baylis–Hillman reaction of ketones and -dicarbonyl compounds
Tadashi Kataoka Hironori Kinoshita Sayaka Kinoshita and Tatsunori Iwamura
pg 2043; DOI:
10.1039/b207646m
PDF
1,2,4-Dithiazolidine-3,5-dione as an isocyanate equivalent in the Mitsunobu reaction
Mark E. Wood Daniel J. Cane-Honeysett and Michael D. Dowle
pg 2046; DOI:
10.1039/b206793e
PDF
2,2,6,6-Tetramethylpiperidin-1-ylthiyl, the sulfur analogue of TEMPO, as an initiator for the controlled radical polymerisation of styrene
Neil Bricklebank and Andrew Pryke
pg 2048; DOI:
10.1039/b206842g
PDF
Synthesis of Boc-protected cis- and trans-4-trifluoromethyl-D-prolines
Xiao-long Qiu and Feng-ling Qing
pg 2052; DOI:
10.1039/b206719f
PDF
The development and application of ruthenium catalysed oxidations of a hydroxamic acid and in situ Diels–Alder trapping of the acyl nitroso derivative
Kevin R. Flower Andrew P. Lightfoot Hayley Wan and Andrew Whiting
pg 2058; DOI:
10.1039/b206430h
PDF
A simple method for the preparation of 3-hydroxyiminodehydroquinate, a potent inhibitor of type II dehydroquinase
Christine Le Sann Chris Abell and Andrew D. Abell
pg 2065; DOI:
10.1039/b206066c
PDF
Tungstate-exchanged Mg-Al-LDH catalyst: an eco-compatible route for the oxidation of sulfides in aqueous medium
B. M. Choudary B. Bharathi Ch. Venkat Reddy and M. Lakshmi Kantam
pg 2069; DOI:
10.1039/b205292j
PDF
Synthesis of a pentasaccharide derivative corresponding to a triterpenoid saponin isolated from Spergularia ramosa
Guofeng Gu and Yuguo Du
pg 2075; DOI:
10.1039/b205106k
PDF
Stereoselective and regioselective synthesis of azepane and azepine derivatives via piperidine ring expansion
Hyun-soon Chong Bishwajit Ganguly Grant A. Broker Robin D. Rogers and Martin W. Brechbiel
pg 2080; DOI:
10.1039/b204677f
PDF
Homologation of -amino acids to -amino acids using Boc2O
Ganga-Ramu Vasanthakumar Basanagoud S. Patil and Vommina V. Suresh Babu
pg 2087; DOI:
10.1039/b204652k
PDF
Elongated phosphoranes by C–C coupling of haloaroylmethylidenetriphenylphosphoranes: synthesis and applications
Thies Thiemann Kuniharu Umeno Jian Wang Yumiko Tabuchi Kazuya Arima Masataka Watanabe Yasuko Tanaka Hideki Gorohmaru and Shuntaro Mataka
pg 2090; DOI:
10.1039/b202745n
PDF
Palladium-mediated synthesis of [carbonyl-11C]amides and hydrazides using [11C]carbon monoxide
Farhad Karimi and Bengt Långström
pg 2111; DOI:
10.1039/b202503e
PDF

Issue 19


Synthesis of terminal monofluoro olefins
Jan Hein van Steenis and Arne van der Gen
pg 2117; DOI:
10.1039/b106187a
PDF
Diastereoselective radical allylation and hydrogenation of -(arylsulfinyl)alkyl radicals induced by chelation control
Nobuyuki Mase Yoshihiko Watanabe Koji Higuchi Shuichi Nakamura and Takeshi Toru
pg 2134; DOI:
10.1039/b207249a
PDF
Palladium-catalyzed tandem C,N-arylation of immobilized enamine for solid phase indole synthesis
Kazuo Yamazaki Yosuke Nakamura and Yoshinori Kondo
pg 2137; DOI:
10.1039/b206378f
PDF
Regioselective synthesis of heterocycles by sigmatropic rearrangement: passage to 3,11a-dimethyl-6a,11a-dihydro-1H,6H-pyrano[3,4:5,6]thiopyrano[4,3-b][1]benzofuran-1-one
Krishna C. Majumdar Uday K. Kundu and Subhojit Ghosh
pg 2139; DOI:
10.1039/b206287a
PDF
Diastereoselective [2,3]-sigmatropic rearrangements of lithium N-benzyl-O-allylhydroxylamides bearing a stereogenic centre adjacent to the migration terminus
Steven D. Bull Stephen G. Davies Sara Hernández Domíngez Simon Jones Anne J. Price Thomas G. R. Sellers and Andrew D. Smith
pg 2141; DOI:
10.1039/b207069n
PDF
Optical resolution and racemization of areneseleninic acids
Toshio Shimizu Yusuke Nakashima Itaru Watanabe Kazunori Hirabayashi and Nobumasa Kamigata
pg 2151; DOI:
10.1039/b206859c
PDF
Synthesis of (R)-6,7-dihydro-5-HETE lactone and (S)-6,7-dihydro-5-HETE lactone by using novel yeast reduction as a key reaction
Satoshi Yamauchi Kenji Takeda Makoto Ganaha and Yoshiro Kinoshita
pg 2156; DOI:
10.1039/b206843p
PDF
Synthesis of nojirimycin C-glycosides
Laura Cipolla Amalia Palma Barbara La Ferla and Francesco Nicotra
pg 2161; DOI:
10.1039/b206623h
PDF
Mechanistic investigations in diastereoselective Diels–Alder additions of chiral 9-anthrylethanol derivatives
J. C. Christian Atherton and Simon Jones
pg 2166; DOI:
10.1039/b206523a
PDF
Synthesis of phosphorylated fragments of Streptococcus pneumoniae type 19F capsular polysaccharide
Giuseppina Soliveri Anna Bertolotti Luigi Panza Laura Poletti Christopher Jones and Luigi Lay
pg 2174; DOI:
10.1039/b205684d
PDF
Synthesis and structural elucidation of 1-(3-C-ethynyl-4-thio--D-ribofuranosyl)cytosine (4-thioECyd)
Noriaki Minakawa Daisuke Kaga Yuka Kato Kanji Endo Motohiro Tanaka Takuma Sasaki and Akira Matsuda
pg 2182; DOI:
10.1039/b204993g
PDF
Elemental fluorine. Part 14. Electrophilic fluorination and nitrogen functionalisation of hydrocarbons
Richard D. Chambers Alan M. Kenwright Mandy Parsons Graham Sandford and John S. Moilliet
pg 2190; DOI:
10.1039/b204776b
PDF
The preparation of polymer beads by photocationic suspension co-polymerisation of 2-(arylsilyl)ethyl vinyl ethers
Laurent Porres Hervé Deleuze and Yannick Landais
pg 2198; DOI:
10.1039/b201520j
PDF

Issue 20


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 20-vii; DOI:
10.1039/b209294h
PDF
Heterogeneous and solid supported dendrimer catalysts
Amy S. H. King and Lance J. Twyman
pg 2209; DOI:
10.1039/b204207j
PDF
O-Glycosylations under neutral or basic conditions
Knud J. Jensen
pg 2219; DOI:
10.1039/b110071h
PDF
Expedient method for the solid-phase synthesis of some 4-substituted-4,5-dihydropyridazin-3(2H)-ones
Nicolas Gouault Jean-François Cupif Maryvonne Amoros and Michèle David
pg 2234; DOI:
10.1039/b205607k
PDF
A mild, enantioselective synthesis of (R)-salmeterol via sodium borohydride–calcium chloride asymmetric reduction of a phenacyl phenylglycinol derivative
Robert N. Bream Steven V. Ley Benjamin McDermott and Panayiotis A. Procopiou
pg 2237; DOI:
10.1039/b207068p
PDF
Total synthesis of (+)-curacin A, a novel antimitotic metabolite from a cyanobacterium
James C. Muir Gerald Pattenden and Tao Ye
pg 2243; DOI:
10.1039/b206796j
PDF
Synthesis and antifouling activity of 3-isocyanotheonellin and its analogues
Yoshikazu Kitano Toshihiro Ito Takehiro Suzuki Yasuyuki Nogata Kyouji Shinshima Erina Yoshimura Kazuhiro Chiba Masahiro Tada and Isamu Sakaguchi
pg 2251; DOI:
10.1039/b206705f
PDF
Palladium-mediated carboxylation of aryl halides (triflates) or benzyl halides using [13C]/[11C]carbon monoxide with tetrabutylammonium hydroxide or trimethylphenylammonium hydroxide
Farhad Karimi and Bengt Långström
pg 2256; DOI:
10.1039/b206420k
PDF
The synthesis of benzylphosphine oxides via vicarious nucleophilic substitution and alkenes via VNS–Horner–Wittig reactions
Nicholas J. Lawrence John Liddle and David Jackson
pg 2260; DOI:
10.1039/b206144a
PDF
Synthesis, structure, and reactivity of (triphenylarsoranylidene)methylcyclohepta-2,4,6-trienone derivatives: reactions with heterocumulenes and an activated acetylene
Yuhki Mitsumoto and Makoto. Nitta
pg 2268; DOI:
10.1039/b205612g
PDF
Synthesis of 16-fluoro ICI 182,780 derivatives: powerful antiestrogens to image estrogen receptor densities in breast cancer by positron emission tomography
Yann Seimbille François Bénard and Johan E. van Lier
pg 2275; DOI:
10.1039/b205571f
PDF
Stereochemically controlled synthesis of substituted 1,2-oxathianes
Jason Eames Nikolai Kuhnert and Stuart Warren
pg 2282; DOI:
10.1039/b205060a
PDF
Hydroxy group interactions in stannylated carbohydrates. Structures and thermal stabilities of 5-deoxy-5-C-(Ph3Sn)-1,2-O-isopropylidene--D-xylofuranose, 5-deoxy-5-C-(IPh2Sn)-1,2-O-isopropylidene--D- and -L-xylofuranose, and 5-deoxy-5-C-(I2PhSn)-1,2-O-isopropylidene--D- and -L-xylofuranose
Lynne A. Burnett Vitor F. Ferreira R. Alan Howie Helena Rufino Janet M. S. Skakle James L. Wardell and Solange M. S. V. Wardell
pg 2288; DOI:
10.1039/b204675j
PDF

Issue 21


Saturated oxygen heterocycles
Mark C. Elliott
pg 2301; DOI:
10.1039/b201515n
PDF
Recent developments in the synthesis of furan-2(5H)-ones
Neil B. Carter Adam E. Nadany and J.B. Sweeney
pg 2324; DOI:
10.1039/b007664n
PDF
Reaction between isocyanides and dialkyl acetylenedicarboxylates in the presence of 3-methylcyclopentane-1,2,4-trione. One-pot diastereoselective synthesis of tetrahydrocyclopenta[b]pyran derivatives
Issa Yavari Mehdi Adib and Mohammad H. Sayahi
pg 2343; DOI:
10.1039/b207548m
PDF
Novel cryptands containing thiourea units as a part of the macrocyclic framework
Nikolay G. Lukyanenko Tatiana I. Kirichenko and Sergey V. Scherbakov
pg 2347; DOI:
10.1039/b207902j
PDF
Nucleophilic addition reactions of bridged triene 6-chromiumtricarbonyl complexes
Rohan E. J. Beckwith Michael B. Gravestock and Nigel S. Simpkins
pg 2352; DOI:
10.1039/b207708f
PDF
Reactions of 2-[(2-arylimino-2-cyano-1,1-dimethylethyl)arylamino]-3-methylbut-2-enenitrile with copper(II) acetate: synthesis of 2-(2,3-dihydro-2,2-dimethyl-3-oxo-1H-indol-1-yl)-3-methylbut-2-enenitriles
Sangmin Yun and Kyongtae Kim
pg 2360; DOI:
10.1039/b207530j
PDF
A flexible synthesis of cyclopentitol derivatives based on ring-closing metathesis of carbohydrate-derived 1,6-dienes
Huib Ovaa Bas Lastdrager Jeroen D. C. Codée Gijs A. van der Marel Herman S. Overkleeft and Jacques H. van Boom
pg 2370; DOI:
10.1039/b207509a
PDF
Chiral oxime ethers in asymmetric synthesis. Part 5. Asymmetric synthesis of 2-substituted 5- to 8-membered nitrogen heterocycles by oxime addition–ring-closing metathesis
James C. A. Hunt Pierre Laurent and Christopher J. Moody
pg 2378; DOI:
10.1039/b207235c
PDF
Dy(OTf)3-immobilized in ionic liquids: a novel and recyclable reaction media for the synthesis of 2,3-unsaturated glycopyranosides
Jhillu. S. Yadav Basi. V. Subba Reddy and J. Shyam Sunder Reddy
pg 2390; DOI:
10.1039/b206957c
PDF
Preparation of deuterium labelled fackel sterols, [5,6,6,7,7,11,11,12,12,15,16,16,17-2Hn]-5-cholesta-8,14-dien-3-ol and its (24R)-24-methyl and -ethyl congeners
Hideharu Seto Keiko Mizukai Shozo Fujioka Hiroyuki Koshino and Shigeo Yoshida
pg 2395; DOI:
10.1039/b206904k
PDF
Chemo-enzymatic preparation of hydroxymethyl ketones
Csaba Paizs Monica Toa Cornelia Majdik Viktória Bódai Lajos Novák Florin-Dan Irimie and László Poppe
pg 2400; DOI:
10.1039/b206851f
PDF
Sequential kinetic resolution of C2-symmetric compounds as a key step in two-directional synthesis: structural requirements for efficient resolution of difuryl diols
Michael Harding Robert Hodgson and Adam Nelson
pg 2403; DOI:
10.1039/b206478b
PDF
Rhodium(II)-mediated reactions of thiobenzoylketene S,N-acetals with -diazo carbonyl compounds: synthesis of 2-substituted 3-alkylamino-5-phenylthiophenes
Hyun Min Song and Kyongtae Kim
pg 2414; DOI:
10.1039/b203931a
PDF

Issue 22


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 22-ix; DOI:
10.1039/b210651p
PDF
1,3-Dipolar cycloaddition reactions of carbohydrate derived nitrones and oximes
Helen M.I. Osborn Natasha Gemmell and Laurence M. Harwood
pg 2419; DOI:
10.1039/b200549m
PDF
A chemoenzymatic synthesis of (–)-hirsutene from toluene
Martin G. Banwell Alison J. Edwards Gwion J. Harfoot and Katrina A. Jolliffe
pg 2439; DOI:
10.1039/b208778b
PDF
Chiral glycine cation equivalents: N-acyliminium species derived from diketopiperazines
Steven D. Bull Stephen G. Davies A. Christopher Garner Michael D. O'Shea Edward D. Savory and Emma J. Snow
pg 2442; DOI:
10.1039/b207457p
PDF
Regioselectivity in the ring-opening -scission of 2-phenyl-1,3-dioxan-2-yl radicals derived from bicyclic benzylidene acetals
Yudong Cai Hai-Shan Dang and Brian P. Roberts
pg 2449; DOI:
10.1039/b208200b
PDF
Extension of the ring switch approach to glutamate antagonists to -lactam urethanes
Diane Coe Martin Drysdale Oliver Philps Robert West and Douglas W. Young
pg 2459; DOI:
10.1039/b207936d
PDF
Halorosellins A and B, unique isocoumarin glucosides from the marine fungus Halorosellinia oceanica
Maneekarn Chinworrungsee Prasat Kittakoop Masahiko Isaka Ratchada Chanphen Morakot Tanticharoen and Yodhathai Thebtaranonth
pg 2473; DOI:
10.1039/b207887m
PDF
Polysaccharide–polynucleotide complexes. Part 12. Enhanced affinity for various polynucleotide chains by site-specific chemical modification of schizophyllan
Kazuya Koumoto Taro Kimura Masami Mizu Toyoki Kunitake Kazuo Sakurai and Seiji Shinkai
pg 2477; DOI:
10.1039/b207553a
PDF
A direct route to conjugated enediynes from dipropargylic sulfones by a modified one-flask Ramberg–Bcklund reaction
Xiaoping Cao Yuying Yang and Xiaolong Wang
pg 2485; DOI:
10.1039/b207296n
PDF
Natural product-derived building blocks for combinatorial synthesis. Part 1. Fragmentation of natural products from myxobacteria
Jutta Niggemann Katrin Michaelis Ronald Frank Norbert Zander and Gerhard Höfle
pg 2490; DOI:
10.1039/b206953a
PDF
Nitrilimine cycloadditions to MeOPEG-bounded alkenyl dipolarophiles
Luisa Garanti Giorgio Molteni and Pietro Casati
pg 2504; DOI:
10.1039/b206629g
PDF
Conformationally locked aryl C-nucleosides: synthesis of phosphoramidite monomers and incorporation into single-stranded DNA and LNA (locked nucleic acid)
B. Ravindra Babu Ashok K. Prasad Smriti Trikha Niels Thorup Virinder S. Parmar and Jesper Wengel
pg 2509; DOI:
10.1039/b206626b
PDF
Desulfurization of thioureas, benzimidazoline-2-thiones and 1,3-dihydro-1,3-diaryl-2-thioxopyrimidine-4,6(2H,5H)-diones with nickel boride at ambient temperature
Jitender M. Khurana Gagan Kukreja and Geeti Bansal
pg 2520; DOI:
10.1039/b206398k
PDF
Origins of stereoselectivity in the chelation-controlled addition of alkyl radicals to -methylene--oxycarboxylic acid esters
Hajime Nagano Satoko Toi Mikako Matsuda Tamano Hirasawa Satomi Hirasawa and Tomoko Yajima
pg 2525; DOI:
10.1039/b205613p
PDF
Asymmetric synthesis of C2-symmetric 5,6-bis(benzyloxy)cyclohexa-1,3-diene and a tricarbonyliron complex
Akiko Watanabe Takao Kamahori Mariko Aso and Hiroshi Suemune
pg 2539; DOI:
10.1039/b205526k
PDF
Regiospecifically deuterated (–)-9-tetrahydrocannabivarins
Spyros P. Nikas Ganesh A. Thakur and Alexandros Makriyannis
pg 2544; DOI:
10.1039/b205459k
PDF
Reactions of -electron rich 1,2,4-triazines with organolithium nucleophiles
Joanna Szczepkowska-Sztolcman Andrzej Katrusiak Hanna Wójtowicz-Rajchel and Krzysztof Golankiewicz
pg 2549; DOI:
10.1039/b205058g
PDF
-Trifluoroacetylvinyl phenyl sulfoxide—synthesis, Diels–Alder reaction and computational study
Arkady L. Krasovsky Serge A. Pissarev Valentine G. Nenajdenko and Elizabeth S. Balenkova
pg 2554; DOI:
10.1039/b202583c
PDF

Issue 23


The modified Julia olefination: alkene synthesis via the condensation of metallated heteroarylalkylsulfones with carbonyl compounds
Paul R. Blakemore
pg 2563; DOI:
10.1039/b208078h
PDF
Nitro and related groups
Joseph P. Adams
pg 2586; DOI:
10.1039/b009711j
PDF
Novel building blocks for crystal engineering: the first synthesis of oligo(imidazole)s
Yasushi Morita Tsuyoshi Murata Satoru Yamada Makoto Tadokoro Akio Ichimura and Kazuhiro Nakasuji
pg 2598; DOI:
10.1039/b208777d
PDF
Tungstophosphoric acid (H3PW12O40) as a heterogeneous inorganic catalyst. Activation of hexamethyldisilazane (HMDS) by tungstophosphoric acid for efficient and selective solvent-free O-silylation reactions
Habib Firouzabadi Nasser Iranpoor Kamal Amani and Farhad Nowrouzi
pg 2601; DOI:
10.1039/b208202k
PDF
Hydrosilylation of cinchonidine and 9-O-TMS-cinchonidine with triethoxysilane: application of 11-(triethoxysilyl)-10,11-dihydrocinchonidine as a chiral modifier in the enantioselective hydrogenation of 1-phenylpropane-1,2-dione
Anna Lindholm Päivi Mäki-Arvela Esa Toukoniitty Tapani A. Pakkanen Janne T. Hirvi Tapio Salmi Dmitry Yu. Murzin Rainer Sjöholm and Reko Leino
pg 2605; DOI:
10.1039/b205032c
PDF
Exploiting multiple nucleophilic sites on pyrrole for the assembly of polyheterocyclic frameworks: application to a formal total synthesis of ()-aspidospermidine
Martin G. Banwell and Jason A. Smith
pg 2613; DOI:
10.1039/b208821e
PDF
Solution phase synthesis of ISIS 2922 (Vitravene) by the modified H-phosphonate approach
Colin B. Reese and Hongbin Yan
pg 2619; DOI:
10.1039/b208802a
PDF
Asymmetric synthesis of tetrahydrofurans by competitive [1,2]-phenylsulfanyl (PhS) migrations under thermodynamic control
Lorenzo Caggiano David J. Fox David House Zoe A. Jones Fraser Kerr and Stuart Warren
pg 2634; DOI:
10.1039/b208556a
PDF
Asymmetric synthesis of tetrahydropyrans with competitive [1,2]-phenylsulfanyl (PhS) migrations
Lorenzo Caggiano David J. Fox David House Zoe A. Jones Fraser Kerr and Stuart Warren
pg 2646; DOI:
10.1039/b208557g
PDF
Scope and limitation of the [1,2]-phenylsulfanyl (PhS) migration in the synthesis of tetrahydrofurans and tetrahydropyrans from common triol precursors
David House Fraser Kerr and Stuart Warren
pg 2652; DOI:
10.1039/b208558e
PDF
Use of sodium triacetoxyborohydride in the synthesis of nitroxide biradicals
Gerald M. Rosen Erika Schneider Sonya Shortkroff Pei Tsai and Carl S. Winalski
pg 2663; DOI:
10.1039/b208263b
PDF
PhSeOTf–Et3N
Helmut Poleschner and Konrad Seppelt
pg 2668; DOI:
10.1039/b207886b
PDF
Synthesis of highly hindered oxepins and an azepine from bis-trityl carbenium ions: structural characterisation by NMR and X-ray crystallography
Kieran A. Carey William Clegg Mark R. J. Elsegood Bernard T. Golding M. N. Stuart Hill and Howard Maskill
pg 2673; DOI:
10.1039/b207108h
PDF
Synthesis of [n]polynorbornanes with differing edge substitution: a new class of regioselectively addressable framework
Frederick M. Pfeffer and Richard A. Russell
pg 2680; DOI:
10.1039/b206057d
PDF
2-Substituted-2,4-endo-dimethyl-8-oxabicyclo[3.2.1]octan-3-ones as catalysts for the asymmetric epoxidation of some alkenes with Oxone
Solange Klein and Stanley M. Roberts
pg 2686; DOI:
10.1039/b205946k
PDF
Synthesis and characterisation of a suite of four chiral pyridyl alcohols derived from (–)-menthol
Desmond Cunningham Eva T. Gallagher David H. Grayson Patrick J. McArdle Christina B. Storey and Deborah J. Wilcock
pg 2692; DOI:
10.1039/b205872n
PDF
Synthesis of N-methyl-N-(1-methylpropyl)-1-(2-chlorophenyl)isoquinoline-3-[11C]carboxamide ([11C-carbonyl]PK11195) and some analogues using [11C]carbon monoxide and 1-(2-chlorophenyl)isoquinolin-3-yl triflate
Obaidur Rahman Tor Kihlberg and Bengt Långström
pg 2699; DOI:
10.1039/b205838c
PDF
Reinvestigation of base-induced skeletal conversion via a spirocyclic intermediate of dibenzodithiocinium derivatives and a computational study using the HF/6-31G* basis set
Keiji Okada and Masato Tanaka
pg 2704; DOI:
10.1039/b205588k
PDF
Isolation and structure of cyclosenegalins A and B, novel cyclopeptides from the seeds of Annona senegalensis
Alassane Wélé Yanjun Zhang Christelle Caux Jean-Paul Brouard Lionel Dubost Catherine Guette Jean-Louis Pousset Mamadou Badiane and Bernard Bodo
pg 2712; DOI:
10.1039/b205035h
PDF
Chemical consequences of fluorine substitution. Part 4. Diels–Alder reactions of fluorinated p-benzoquinones with Dane's diene. Synthesis of fluorinated D-homosteroids
Michael Essers and Günter Haufe
pg 2719; DOI:
10.1039/b208001j
PDF

Issue 24


Perkin 1 Abstracts: Biocatalysis in Organic Synthesis
Gideon Grogan Selena Guilly Ian Jackson Denise McIntyre Reuben Carr Sabine Flitsch and Nicholas Turner
pg 22-xv; DOI:
10.1039/b211566m
PDF
The Sharpless asymmetric aminohydroxylation
Jennifer A. Bodkin and Malcolm D. McLeod
pg 2733; DOI:
10.1039/b111276g
PDF
Synthesis of heterocycles by radical cyclisation
W. Russell Bowman Anthony J. Fletcher and Graeme B. S. Potts
pg 2747; DOI:
10.1039/b108582b
PDF
Titanium reagents for the alkylidenation of carboxylic acid and carbonic acid derivatives
Richard C. Hartley and Gordon J. McKiernan
pg 2763; DOI:
10.1039/b009709h
PDF
Nitroalkanes as nucleophiles in a self-catalytic Michael reaction
Henryk Krawczyk Wojciech M. Wolf and Marcin liwiski
pg 2794; DOI:
10.1039/b209302m
PDF
A facile route to pyrroles, isoindoles and hetero fused analogues
Christopher D. Gabbutt John D. Hepworth B. Mark Heron and Samantha L. Pugh
pg 2799; DOI:
10.1039/b209255g
PDF
Fluorination of -phenylsulfanyl esters using difluoroiodotoluene
William B. Motherwell Michael F. Greaney and Derek A. Tocher
pg 2809; DOI:
10.1039/b209079a
PDF
Fluorination of sulfanyl amides using difluoroiodoarene reagents
William B. Motherwell Michael F. Greaney Jeremy J. Edmunds and Jonathan W. Steed
pg 2816; DOI:
10.1039/b209078c
PDF
New ligands for asymmetric diethylzinc additions to aromatic aldehydes, demonstrating substrate-dependent nonlinear effects
Philip C. Bulman Page Steven M. Allin Suzanne J. Maddocks and Mark R. J. Elsegood
pg 2827; DOI:
10.1039/b208810j
PDF
Stereocontrolled synthesis of glucosidic damascenone precursors
Yumiko Yamano Yasuko Watanabe Naoharu Watanabe and Masayoshi Ito
pg 2833; DOI:
10.1039/b208758h
PDF
Palladium(0) catalysed and copper(I) promoted reactions of the secondary zinc reagent derived from L-threonine
Ian Wilson and Richard F. W. Jackson
pg 2845; DOI:
10.1039/b208667k
PDF
A new tricyclic ring and a nitrogen–sulfur analogue of the tri-pentagon bowl: cycloaddition reactions of the unstablised 1,3,4-thiadiazolium-3-methanide 1,3-dipole: steric influences on the endo-effect: substituted pyrrolo[2,1-b]-1,3,4-thiadiazole systems: azolium 1,3-dipoles
Richard N. Butler Georgina M. Smyth Patrick McArdle and Desmond Cunningham
pg 2851; DOI:
10.1039/b208544p
PDF
In situ IR and NMR spectroscopic investigation of the formation and structure of protonated diacetylketene tetrachloroaluminate
Szilárd Csihony Andrea Bodor János Rohonczy and István T. Horváth
pg 2861; DOI:
10.1039/b208387f
PDF
Comparative study of base damage induced by gamma radiation and Fenton reaction in isolated DNA
Sandrine Frelon Thierry Douki Alain Favier and Jean Cadet
pg 2866; DOI:
10.1039/b207532f
PDF
Synthesis of ,-disubstituted unnatural amino acid derivatives using the aza-[2,3]-Wittig sigmatropic rearrangement
James C. Anderson and Sarah Skerratt
pg 2871; DOI:
10.1039/b207295e
PDF
Unusual hydrogen-bonding differences in stereoisomeric 6-C-alkylated cyclodextrins
Tore Hardlei and Mikael Bols
pg 2880; DOI:
10.1039/b207033m
PDF
Synthesis and optimization of tri(propylene glycol) glycerolate diacrylate cross-linked polystyrene resin in polypeptide synthesis: role of the macromolecular support in solid phase peptide synthesis
P. G. Sasikumar K. S. Kumar C. Arunan and V. N. Rajasekharan Pillai
pg 2886; DOI:
10.1039/b206879f
PDF
A nucleophilic addition ring closure [NARC]-based synthesis of (+) -nonactic acid
Benjamin Fraser and Patrick Perlmutter
pg 2896; DOI:
10.1039/b206656d
PDF
Novel preparation of non-racemic 1-[-(1-azacycloalkyl)benzyl]-2-naphthols from Betti base and their application as chiral ligands in the asymmetric addition of diethylzinc to aryl aldehydes
Jun Lu Xuenong Xu Shaozhong Wang Cunde Wang Yuefei Hu and Hongwen Hu
pg 2900; DOI:
10.1039/b204534f
PDF